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Process for preparing catalyst composition for the synthesis of carbon nanotube with high yields using the spray pyrolysis method

机译:使用喷雾热解法制备高产率合成碳纳米管的催化剂组合物的方法

摘要

The invention carbon nanotubes; relates to a process for preparing (Carbon Nanotube CNT) composite catalyst composition. More specifically, the present invention is one of the main catalytic metal selected from Fe or Co; Al; Fe, Co, Ni, Cu, Sn, Mo, Cr, Mn, V, W, Ti, Si, Zr, at least one metal selected from crude Y catalyst; And a process for producing a multi-component metal catalyst composition comprising an inert support Mg, by dissolving the precursor of the metal catalyst composition in water to prepare a catalyst mixed solution, the reactor of the high temperature to the catalyst mixture as a gas atomizing method sikimyeo by spraying a high-temperature pyrolysis to form a catalyst powder, and a method for producing a catalyst composition for synthesizing carbon nanotubes using the spray pyrolysis method consisting of a step of obtaining the catalyst powder. The carbon nanotube composite catalyst composition prepared by the method has a very low apparent density of 0.01~0.50g / mL can be prepared in a high yield of carbon nanotubes Yield 1000~1800%.
机译:发明碳纳米管;本发明涉及一种制备(碳纳米管CNT)复合催化剂组合物的方法。更具体地说,本发明是选自Fe或Co的主要催化金属之一。铝Fe,Co,Ni,Cu,Sn,Mo,Cr,Mn,V,W,Ti,Si,Zr,至少一种选自粗制Y催化剂的金属;以及一种制备包含惰性载体Mg的多组分金属催化剂组合物的方法,该方法是通过将金属催化剂组合物的前体溶解在水中以制备催化剂混合溶液,将高温反应器以气体雾化的方式加入到催化剂混合物中喷射高温热解以形成催化剂粉末的方法,以及使用喷雾热解法制备用于合成碳纳米管的催化剂组合物的方法,该方法包括获得催化剂粉末的步骤。通过该方法制备的碳纳米管复合催化剂组合物具有非常低的表观密度为0.01〜0.50g / mL,可以制备出高产率的碳纳米管,产率为1000〜1800%。

著录项

  • 公开/公告号KR101241034B1

    专利类型

  • 公开/公告日2013-03-11

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20100076674

  • 申请日2010-08-10

  • 分类号B01J23/889;B01J23/881;B01J37/12;B82B3/00;

  • 国家 KR

  • 入库时间 2022-08-21 16:25:34

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