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METHOD FOR DETECTING POLLUTION OF TITANIUM ALLOYS OF TWO-PHASE TYPE WITH ALPHA AND BETA-PHASE

机译:α和β相检测两相钛合金污染的方法

摘要

1. A method for studying a two-phase type titanium alloy with an alpha phase and a beta phase, characterized in that it includes the following steps: (a) a sample is cut from a part from said alloy; (b) a region (4) of a cut surface of said sample is prepared, located near the edge (50) of said sample, said edge (50) being in common with the outer surface (1) of the part, so as to allow examination of said region (4); (c) the alpha phase of said region (4) is examined at more than 5,000-fold magnification; (d) decide whether granularity is present or absent in the alpha phase of the first zone (11) adjacent to said edge (50) of the sample; (e) conclude that there is gas contamination of the alloy, if established the absence of graininess in the alpha phase of said adjacent zone (11), while graininess (22) is present in the alpha phase outside said adjacent zone (11) .2. A method for studying a titanium alloy according to claim 1, characterized in that said examination at step (c) is carried out using a scanning electron microscope. A method for researching a titanium alloy according to claim 1 or 2, characterized in that the preparation of said region (4) in step (b) involves polishing said region (4) and then chemically etching said region (4) with at least one reagent. . A method for researching a titanium alloy according to claim 3, characterized in that said chemical etching is carried out by a single reagent. The research method for a titanium alloy according to claim 4, characterized in that said reagent is an aqueous solution of hydrofluoric acid HF with a concentration of 0.5%
机译:1.一种研究具有α相和β相的两相型钛合金的方法,其特征在于,它包括以下步骤:(a)从所述合金的一部分上切下样品; (b)制备所述样品的切割表面的区域(4),其位于所述样品的边缘(50)附近,所述边缘(50)与所述部件的外表面(1)相同,从而允许检查所述区域(4); (c)以大于5,000倍的放大倍数检查所述区域(4)的α相; (d)确定在与样品的所述边缘(50)相邻的第一区域(11)的α相中是否存在粒度; (e)得出结论,如果确定在所述相邻区域(11)的α相中不存在粒状,而在所述相邻区域(11)之外的α相中存在粒状(22),则存在合金的气体污染。 2。 2.根据权利要求1的研究钛合金的方法,其特征在于,步骤(c)中的所述检查是使用扫描电子显微镜进行的。 3.根据权利要求1或2所述的研究钛合金的方法,其特征在于,在步骤(b)中制备所述区域(4)包括抛光所述区域(4),然后用至少一个化学蚀刻所述区域(4)。试剂。 。 4.根据权利要求3所述的研究钛合金的方法,其特征在于,所述化学蚀刻通过单一试剂进行。 5.根据权利要求4所述的钛合金的研究方法,其特征在于,所述试剂是浓度为0.5%的氢氟酸HF的水溶液。

著录项

  • 公开/公告号RU2012111839A

    专利类型

  • 公开/公告日2013-10-10

    原文格式PDF

  • 申请/专利权人 СНЕКМА (FR);

    申请/专利号RU20120111839

  • 发明设计人 БЕРТО ЖИЛЛЬ (FR);

    申请日2010-07-27

  • 分类号G01N33/20;

  • 国家 RU

  • 入库时间 2022-08-21 16:23:32

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