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METHOD OF GROWING LITHIUM-MAGNESIUM MOLYBDATE MONOCRYSTALS

机译:钼酸锂镁单晶的生长方法

摘要

FIELD: chemistry.;SUBSTANCE: invention relates to the technology of growing lithium-magnesium molybdate Li2Mg2(MoO4)3 crystals. The method involves melting lithium-magnesium molybdate in a molten solvent, crystallising while cooling the melt and cooling the grown crystals, wherein the solvent used is lithium molybdate Li2MoO4 with molar ratio of lithium-magnesium molybdate to lithium molybdate Li2MoO4 of 2:3, respectively; crystallisation is carried out on an inoculating crystal revolving at a rate of 35 rpm, oriented on the [010] direction, rate of drawing rate of the inoculating crystal of 1-3 mm/day while simultaneously cooling the melt at a rate of 0.2-5 degrees/day and then separating the grown crystals from the melt and cooling at a rate of 30 degrees/hour.;EFFECT: method enables to obtain optically homogeneous lithium-magnesium molybdate crystals which do not contain inclusions, blocks and cracks.
机译:锂镁钼酸锂Li 2 Mg 2 (MoO 4 的生长技术3 晶体。该方法包括在熔融溶剂中熔融钼酸锂镁,在冷却熔体的同时结晶并冷却生长的晶体,其中使用的溶剂为钼酸锂Li 2 MoO 4 钼酸锂镁与钼酸锂Li 2 MoO 4 的摩尔比分别为2:3;在以[101]方向定向的35 rpm转速旋转的接种晶体上进行结晶,接种晶体的拉伸速率为1-3 mm /天,同时以0.2-每天5度,然后将生长的晶体从熔体中分离出来,并以30度/小时的速度冷却。效果:该方法能够获得光学均质的钼酸锂镁晶体,其中不含夹杂物,块和裂纹。

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