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Method for preparing pyrochlore oxide catalyst and method for producing electrode catalyst for fuel cell

机译:制备烧绿石氧化物催化剂的方法和制备用于燃料电池的电极催化剂的方法

摘要

A pyrochlore-type oxide represented by a general formula A2B2O7-Z is prepared by precipitate formation, where A and B each represent a metal element, where Z represents a number of at least 0 and at most 1, where A contains at least one element selected from a group consisting of Pb, Sn, and Zn, and where B contains at least one element selected from a group consisting of Ru, W, Mo, Ir, Rh, Mn, Cr, and Re. Impurities are then sufficiently removed through washing and drying processes, and the pyrochlore-type oxide is calcined under controlled conditions. This allows the crystallinity of the pyrochlore-type oxide, which contained amorphous parts immediately after the production of the precipitate, to be increased so that the resistance to acid can be improved while preventing particle aggregation.
机译:通过沉淀形成来制备由通式A2B2O7-Z表示的烧绿石型氧化物,其中A和B各自表示金属元素,其中Z表示至少0且至多1的数目,其中A包含至少一种元素。选自由Pb,Sn和Zn组成的组中,并且其中B包含选自由Ru,W,Mo,Ir,Rh,Mn,Cr和Re组成的组中的至少一种元素。然后通过洗涤和干燥过程充分去除杂质,并在受控条件下煅烧烧绿石型氧化物。这使得在沉淀物刚产生后立即包含非晶态部分的烧绿石型氧化物的结晶度增加,从而可以在防止颗粒聚集的同时提高耐酸性。

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