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HIGH-TEMPERATURE FURNACE, USE OF A SPINEL CERAMIC AND METHOD FOR CARRYING OUT T(O)C MEASUREMENTS OF SAMPLES

机译:高温炉,尖晶石陶瓷的使用以及进行样品T(O)C测量的方法

摘要

The present invention relates to a high-temperature furnace for T(O)C measurement of a sample, which has a furnace housing which bounds a vaporization space and has a sample opening for the dropwise introduction of the sample and at least one flushing opening for introduction of a flushing liquid. According to the invention, the furnace housing is lined with a spinel ceramic on an inner side facing the vaporization space. By means of the spinel ceramic, the vaporization space is lined with a material which allows particularly high temperatures within the vaporization space and thus very complete combustion and is at the same time very resistant to temperature changes. This allows cleaning with a flushing liquid at essentially the operating temperature of the vaporization space and removal of deposited salts, in particular recrystallized organic salts, from the vaporization space in the flushing liquid in dissolved or undissolved form. Aging of the high-temperature furnace by deposited salts can thereby be avoided or at least significantly retarded.
机译:用于样品的T(O)C测量的高温炉技术领域本发明涉及一种用于样品的T(O)C测量的高温炉,该高温炉具有限定气化空间的炉壳,并具有用于逐滴引入样品的样品开口和至少一个用于冲洗样品的冲洗开口。引入冲洗液。根据本发明,炉壳在面对汽化空间的内侧衬有尖晶石陶瓷。借助于尖晶石陶瓷,在汽化空间内衬有一种材料,该材料在汽化空间内允许特别高的温度,从而非常完全地燃烧,并且同时非常耐温度变化。这允许基本上在汽化空间的操作温度下用冲洗液进行清洁,并且从溶解或未溶解形式的冲洗液中的汽化空间中除去沉积的盐,特别是重结晶的有机盐。由此可以避免或至少显着地阻止高温炉通过沉积的盐老化。

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