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METHOD FOR SYNTHESIS OF CARBON-BASED CATALYST AND ITS APPLICATION FOR BIODIESEL PRODUCTION

机译:碳基催化剂的合成方法及其在生物柴油生产中的应用

摘要

The present invention relates to an acquisition method of a new sulfonated carbon-based catalyst and its further application for biodiesel synthesis. This catalyst is obtained from cellulose in a one stage process where cellulose partial carbonization as well as sulfonation occurs simultaneously. Conseqyently, this produces a mesoporous amorphous carbon matrix with the properties of an acidic heterogeneous catalyst. Sulfonated carbon based catalyst exhibits a high catalytic activity for esterification reaction of fatty acids. A maximum yield of 97 % was achieved in fatty acid esterification reaction with methanol. This invention can be used for a direct one stage biodieselporoduction process where as the first stage is an esterification of fatty acids but second stage is an alkaline transesterification of triglycerides.
机译:本发明涉及一种新型磺化碳基催化剂的获取方法及其在生物柴油合成中的进一步应用。该催化剂是在一个阶段的过程中从纤维素制得的,其中纤维素部分碳化和磺化同时发生。因此,这产生了具有酸性非均相催化剂性质的中孔无定形碳基质。磺化碳基催化剂对脂肪酸的酯化反应显示出高催化活性。与甲醇的脂肪酸酯化反应中,最大产率为97%。本发明可用于直接的一步生物柴油穿孔工艺,其中第一步是脂肪酸的酯化反应,而第二步是甘油三酸酯的碱性酯交换反应。

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