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METHOD FOR THE DETERMINATION OF CHLOROPYRAMINE HYDROCHLORIDE BY GAS-LIQUID CHROMATOGRAPHY

机译:气相色谱法测定盐酸氯丁胺的方法

摘要

Disclosed is a method for the determination of chloropyramine hydrochloride by gas-liquid chromatography according to preset temperature program. Mixture of 5%-diphenyl-95%-dimethyl polysiloxane, HP-5 0.25 µm is used as a stationary liquid phase, and column temperature is linearly programmed in such a way: for 5 min. followed by temperature increment up to with rate of per min.; temperature increment from 200 to with rate of per min. and maintaining at level of for 6 min., and the temperature of evaporator and detector doesnt exceed .
机译:公开了一种根据预设温度程序通过气液色谱法测定盐酸氯吡胺的方法。将5%-二苯基-95%-二甲基聚硅氧烷HP-5 0.25 µm的混合物用作固定液相,并对色谱柱温度进行线性编程:5分钟。然后以每分钟的速度升高温度;温度从200升至每分钟的速率。并保持在6分钟的水平,并且蒸发器和检测器的温度不超过。

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