首页> 外国专利> Procedure for obtaining hydroxytyrosol extract, extract mixture of hydroxytyrosol and 3,4-dihydroxyphenylglycol, and hidroxitirosilo acetate extract, from by-products of the olive and its purification.

Procedure for obtaining hydroxytyrosol extract, extract mixture of hydroxytyrosol and 3,4-dihydroxyphenylglycol, and hidroxitirosilo acetate extract, from by-products of the olive and its purification.

机译:从橄榄的副产物中获得羟基酪醇提取物,羟基酪醇和3,4-二羟基苯基乙二醇的混合物的提取物以及醋酸Hidroxitirosilo提取物的步骤及其提纯方法。

摘要

Procedure for obtaining hydroxytyrosol extract, extract mixture of hydroxytyrosol and 3,4-dihydroxyphenylglycol, and hidroxitirosilo acetate extract, from by-products of the olive and its purification. # Procedure for obtaining an extract comprising hydroxytyrosol, well as acetylated product or as a mixture with 3.4 dihydroxyphenylglycol and purification of all of them, comprising at least one column chromatography a source of hydroxytyrosol as byproducts of olives and olive using a mixture of at least two ionic resins preferably an anionic resin with a cationic resin. Preferably in a first stage a mixture Hydroxytyrosol 3-4-dihydroxyphenylglycol (DHFG a liquid rich source of phenols is obtained as raw material for the extraction and purification of phenolic compounds, a second phase allows to obtain an enriched hydroxytyrosol (HT) extract ) and ethyl hidroxitirosilo occurs, obtaining in the third very pure hydroxytyrosol phase, the DHFG, their mixture and ethyl HT. Each phase comprises extraction, reaction, concentration, adsorption and desorption using mixtures of ion exchange resins, adsorption resins and nonionic polymeric phenolic fraction, reverse osmosis membranes and / or evaporators.
机译:从橄榄的副产物中获得羟基酪醇提取物,羟基酪醇和3,4-二羟基苯基乙二醇的混合物的提取物以及醋酸Hidroxitirosilo提取物的步骤及其提纯方法。 #获得包含羟基酪醇,乙酰化产物或与3.4二羟基苯基乙二醇的混合物的提取物并纯化所有步骤的程序,包括至少一个柱色谱法,使用至少两种的混合物,作为橄榄和橄榄副产物的羟基酪醇源离子树脂优选为阴离子树脂和阳离子树脂。优选地,在第一阶段中,获得羟基酪醇3-4-4-二羟基苯基乙二醇的混合物(DHFG,富含液体的酚源)作为用于酚类化合物的提取和纯化的原料,第二阶段允许获得富集的羟基酪醇(HT)提取物)和出现乙基高铁基噻吩并在第三非常纯的羟基酪醇相中获得DHFG,它们的混合物和乙基HT。每个阶段包括使用离子交换树脂,吸附树脂和非离子聚合酚类馏分,反渗透膜和/或蒸发器的混合物进行萃取,反应,浓缩,吸附和解吸。

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