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METHOD OF ATOMIC ABSORPTION ANALYSIS AND ATOMIC ABSORPTION PHOTOMETER

机译:原子吸收分析方法及原子吸收光度计

摘要

Provided is an atomic absorption photometer with which a liquid measurement sample injected into a graphite tube is dried in a pre-measurement stage, wherein it is possible to determine whether the drying has been properly executed, and wherein a targeted measurement sensitivity and measurement reproducibility are provided with a minimum number of measurements and without many repetitions of measurement. The present invention comprises finding the absorbance of reference light, which is a component perpendicular to a magnetic field in light transmitted through a heating section, and determining there to be bumping of a sample if the duration of time where the absorbance of the reference light is greater than a predetermined value is within a predetermined duration of time; or alternatively finding the absorbance of sample light, which is a component parallel to a magnetic field in light transmitted through the heating section, and the absorbance of reference light, which is a component perpendicular to the magnetic field in light transmitted through the heating section, and determining there to be bumping of a sample if a corrected absorbance obtained by subtracting the reference light absorbance from the sample light absorbance is greater than a predetermined value.
机译:提供一种原子吸收光度计,利用该原子吸收光度计可以在预测量阶段对注入到石墨管中的液体测量样品进行干燥,其中可以确定干燥是否已经正确执行,并且其中目标测量灵敏度和测量再现性达到目标。提供最少的测量次数,并且无需多次重复测量。本发明包括找到参考光的吸收率,该吸收率是垂直于通过加热部分的光中的磁场的分量,并且如果参考光的吸收率的持续时间为0,则确定样品存在碰撞。大于预定值是在预定的持续时间内;或者找到样品光的吸光度,其为平行于通过加热部的光中的磁场的分量;以及参考光的吸光度,其为垂直于通过加热部中的光的磁场的分量,如果从样品吸光度中减去基准吸光度而得到的校正吸光度大于预定值,则判断样品存在碰撞。

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