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Method of Producing Organo-Sericite for Removing Cu(II) in Waste Water

机译:生产有机绢云母去除废水中Cu(II)的方法

摘要

PURPOSE: A manufacturing method of organic-sericite is provided to be able to manufacture organic-sericite having a good copper ion adsorption effect in a shortened period, and to prepare a ground that the organic-sericite product is able to be industrially produced and utilized through an improved manufacturing method. CONSTITUTION: Organic-sericite for adsorbing and removing the copper element in wastewater is manufactured by processing the surface of sericite and forming a micro void between layers by using a mercapto silane compound, separating and drying to obtain organic-sericite particles. The mercapto silane compound is 3-mercaptopropyltrimethoxysilane. A manufacturing method of organic-sericite comprises a process of manufacturing a sericite solution by putting 10 g of sericite and 200-300 ml of toluene as a reaction co-solvent within a sealed container, forming a firstly homogeneous solution state with stirring, adding 15-25 ml of 3-mercaptopropyltrimethoxylsilane to the solution, ion-exchanging by stirring at a high temperature of 60-70deg.C for 10-14 hours and cooling to a room temperature; a process of separating pure organic-sericite by pouring the ion-exchanged sericite solution on a filter medium and repeatedly pouring toluene as a washing agent to wash; and a process of obtaining organic-sericite particles by removing residual toluene in an oven of 100-110deg.C for 2-4 hours.
机译:用途:提供一种有机绢云母的制造方法,以能够在短时间内制造具有良好的铜离子吸附效果的有机绢云母,并为有机绢云母产品能够工业化生产和利用奠定基础。通过改进的制造方法。组成:用于吸附和去除废水中铜元素的有机绢云母是通过处理绢云母的表面并使用巯基硅烷化合物在各层之间形成微空隙,分离并干燥以获得有机绢云母颗粒而制造的。巯基硅烷化合物是3-巯基丙基三甲氧基硅烷。有机绢云母的制造方法包括以下步骤:通过将10g绢云母和200-300ml甲苯作为反应助溶剂放入密封容器中,在搅拌下形成第一均匀溶液状态,从而制备绢云母溶液。将-25ml 3-巯基丙基三甲氧基硅烷加到溶液中,通过在60-70℃的高温下搅拌10-14小时并冷却至室温进行离子交换;通过将离子交换的绢云母溶液倒在过滤介质上并反复倒入甲苯作为洗涤剂来分离纯有机绢云母的方法;通过在100-110℃的烘箱中除去残留的甲苯2-4小时而获得有机绢云母颗粒的方法。

著录项

  • 公开/公告号KR101337987B1

    专利类型

  • 公开/公告日2013-12-06

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20120022872

  • 发明设计人 이승목;김무늬;

    申请日2012-03-06

  • 分类号B01J20/32;B01J20/10;C01G3;B09B3;

  • 国家 KR

  • 入库时间 2022-08-21 15:44:06

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