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Manufacturing method of adsorbent based on magnetic nanoparticles for radioactive cesium

机译:基于磁性纳米粒子的放射性铯吸附剂的制备方法

摘要

The present invention relates to a manufacturing method of an adsorbent for eliminating radioactive cesium based on a magnetic manoparticle and, more specifically, to the manufacturing method of the adsorbent for eliminating the radioactive cesium in which ferrocyanide is combined to the surface of the magnetic manoparticle, and an adsorbent manufactured thereby. The manufacturing method of the adsorbent for eliminating the radioactive cesium comprises a step (1) of adding an iron compound and a first solvent in a reactor and after increasing the same with a high temperature and manufacturing a magnetic manoparticle by a thermal decomposition method, reducing the temperature inside the reactor to a room temperature and obtaining the magnetic manoparticle by eliminating a non-react and the fist solvent; a step (2) of adding a second solvent and a silane coupling agent in the magnetic manoparticle obtained in the step (1) and increasing the same with a high temperature and reacting the same and obtaining a reacted result and eliminating and drying a non-react and the second solvent and obtaining a reacted result of powder type; a step (3) of adding the reacted result obtained in the step (2) in distilled water and putting a metal ion in the distilled water and reacting the same at room temperature and adding overwater and cleaning the same and collecting the magnetic manoparticle using a magnetic field; and a step (4) of adding the magnetic manoparticle collected in the step (2) in distilled water and putting ferrocyanide in the distilled water and reacting the same.
机译:本发明涉及一种基于磁性磁性微粒的用于去除放射性铯的吸附剂的制造方法,更具体地,涉及一种在磁性磁性微粒的表面结合有亚铁氰化物的用于去除放射性铯的吸附剂的制造方法,以及由此制造的吸附剂。用于消除放射性铯的吸附剂的制造方法包括以下步骤:(1)在反应器中添加铁化合物和第一溶剂,并在将其高温升高后通过热分解法制造磁性曼诺颗粒,还原将反应器内的温度升至室温,并通过消除未反应的溶剂和第一溶剂得到磁性的磁性粒子。步骤(2),将第二溶剂和硅烷偶联剂加入步骤(1)中获得的磁性纳米粒子中,并在高温下使其升高并使之反应,从而获得反应结果,并消除和干燥非-与第二溶剂发生反应,得到粉末状的反应结果。步骤(3),将步骤(2)中获得的反应结果添加到蒸馏水中,将金属离子放入蒸馏水中,使其在室温下反应,并加水洗涤并收集,并使用磁场;步骤(4)是将步骤(2)中收集的磁性磁性微粒加入蒸馏水中,然后将亚铁氰化物放入蒸馏水中并使之反应。

著录项

  • 公开/公告号KR101429560B1

    专利类型

  • 公开/公告日2014-08-12

    原文格式PDF

  • 申请/专利权人

    申请/专利号KR20130003314

  • 发明设计人 양희만;이근우;서범경;문제권;

    申请日2013-01-11

  • 分类号G21F9/12;

  • 国家 KR

  • 入库时间 2022-08-21 15:40:19

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