首页> 外国专利> SORBENT- DETONATION NANODIAMOND-CONTAINING MATERIALS, METHOD OF OBTAINING IMMUNOSORBENTS ON THEIR BASIS AND THE IMMUNOSORPTIONS

SORBENT- DETONATION NANODIAMOND-CONTAINING MATERIALS, METHOD OF OBTAINING IMMUNOSORBENTS ON THEIR BASIS AND THE IMMUNOSORPTIONS

机译:含爆炸爆轰的含纳米金刚石材料,基于其获得免疫吸附剂的方法和免疫吸附

摘要

1. nanodiamond materials - products of detonation synthesis mixture produced by the explosion of TNT and RDX at the optimum ratio of 50/50 at a pressure of 16-23 GPa and a temperature of about 3000 K, containing individual particles with a size of 5 nm to form aggregates of varying size 300 nm, comprising or blend, or nanodiamond or nanodiamond modification, as a sorbent for the removal of viruses, viral DNA and antibody fragments, non-viral proteins and for their immunosorbent osnove.2. Sorbents according to claim 1, obtained by liquid-phase batch purification in dilute nitric acid at a pressure of about 80 atm and a temperature of ~ 220 ° C, followed by a multistage washing of nanodiamonds from an acid, wherein the pH of the slurry at a concentration of 6.2 nanodiamonds 1 g / l .3. Sorbents according to claim 1, obtained by gas-phase batch purification in the nitric acid vapor at temperature up to 300 ° C followed by purification of nanodiamonds from non-carbon impurities in a stream of dry hydrogen chloride at a temperature of 850 ° C wherein the pH of suspensions at a concentration of 5 g 1 nanodiamonds /l.4. Sorbents according to claim 1, in the form graphitized detonation nanodiamond obtained by modifying the sorbents according to Claim 2 by heating at high purity argon at T = 1000 ° C for 1 hour, causing a partial phase transition of diamond - grafit.5. Sorbents according to claim 1, in the form of chlorinated detonation nanodiamond obtained by modifying the sorbents according to claim 3, by heating at a temperature T = 450 ° C for 2 hours in a steam-gas CCl / Ar mixture containing 3% by volume CCl.6 . Sorbents according to claim 1, in the form of detonation aminated nanodiamond obtained in the p
机译:1.纳米金刚石材料-在16-23 GPa的压力和约3000 K的温度下,以50/50的最佳比例爆炸TNT和RDX产生的爆炸合成混合物的产品,其中包含5个单独的颗粒1纳米以形成300纳米大小的聚集体,包括或掺合或纳米金刚石或纳米金刚石修饰,作为去除病毒,病毒DNA和抗体片段,非病毒蛋白及其免疫吸附剂的吸附剂。2。 2.根据权利要求1所述的吸收剂,其通过以下方式获得:在约80atm的压力和约220℃的温度下在稀硝酸中进行液相间歇纯化,然后从酸中分步洗涤纳米金刚石,其中所述浆料的pH为浓度为6.2纳米金刚石1 g / l.3。 2.根据权利要求1所述的吸收剂,其通过以下方式获得:在最高300℃的温度下在硝酸蒸气中进行气相间歇纯化,然后在850℃的干燥氯化氢流中从非碳杂质中纯化纳米金刚石。悬浮液的pH值为5 g 1纳米金刚石/l.4。 6.根据权利要求1的吸收剂,为石墨化爆轰纳米金刚石的形式,其通过将根据权利要求2的吸收剂通过在T = 1000℃下在高纯度氩气下加热1小时而改性,从而引起金刚石-涂鸦的部分相变而获得。5。 3.根据权利要求1的吸附剂,其为通过将根据权利要求3的吸附剂改性而得到的氯化爆炸纳米金刚石的形式,该吸附剂通过在温度T = 450℃下在含有3体积%的蒸汽-CCl / Ar混合物中加热2小时而获得。 CCl.6。 2.根据权利要求1的吸附剂,其为在p中获得的爆炸胺化纳米金刚石的形式。

相似文献

  • 专利
  • 外文文献
  • 中文文献
获取专利

客服邮箱:kefu@zhangqiaokeyan.com

京公网安备:11010802029741号 ICP备案号:京ICP备15016152号-6 六维联合信息科技 (北京) 有限公司©版权所有
  • 客服微信

  • 服务号