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PROCESS FOR SYNTHESIZING HYBRIDE BIFUNCTIONALIZED MULTIWALLED CARBON NANOTUBES AND APPLICATIONS THEREOF

机译:氢化物双官能化碳纳米管的合成方法及其应用

摘要

The present disclosure provides a process for synthesizing functionalized multi-walled carbon nanotubes (MWCNTs), comprising: refluxing MWCNTs with an acidic mixture to obtain a acid functionalized MWCNTs; and reacting the acid functionalized MWCNTs with oleyl amine in presence of an organic solvent to obtain an oleylamine derivative of MWCNTs. The present disclosure also provides a process for synthesizing a polycarbosilane coated MWCNT, comprising: mixing polycarbosilane and MWCNTs to obtain a mixture; stirring the mixture in Tetrahydrofuran, in presence of a catalyst under an inert atmosphere, to obtain a reaction mixture; and drying the reaction mixture under vacuum followed by heating to obtain polycarbosilane coated MWCNT's. The present disclosure further provides the application of functionalized MWCNTs as synthesized in accordance with the present disclosure, for use in making photovoltaic devices and the application of polycarbosilane coated MWCNTs as synthesized in accordance with the present disclosure for use in making glass fiber reinforced epoxy composites.
机译:本公开提供了一种合成官能化多壁碳纳米管(MWCNT)的方法,该方法包括:将MWCNT与酸性混合物回流以获得酸官能化的MWCNT;使酸官能化的MWCNT与油胺在有机溶剂的存在下反应,得到MWCNT的油胺衍生物。本公开还提供了一种合成聚碳硅烷涂覆的MWCNT的方法,该方法包括:混合聚碳硅烷和MWCNT以获得混合物;和在惰性气氛下,在催化剂的存在下,将该混合物在四氢呋喃中搅拌,得到反应混合物。真空干燥反应混合物,然后加热,得到聚碳硅烷包覆的MWCNT。本发明进一步提供了根据本发明合成的官能化的MWCNT在制造光伏器件中的应用以及根据本发明合成的聚碳硅烷涂覆的MWCNT在制造玻璃纤维增​​强的环氧复合材料中的应用。

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