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Borosilicate luminescent material and preparing method thereof
Borosilicate luminescent material and preparing method thereof
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机译:硼硅酸盐发光材料及其制备方法
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摘要
Provided are a luminescent material and a preparing method thereof. The borosilicate luminescent material has a chemical formula of aM2O.bLn2O3.cAl2O3.dR2O3.eSiO2.fCeO2.gTb2O3 or aMO.bLn2O3.cAl2O3.dR2O3.eSiO2.fCeO2.gTb2O3, wherein M is alkaline earth metal or alkali metal, Ln is one or two elements selected from the group consisting of elements Y and Gd; R is one or two elements selected from the group consisting of elements B and P; a, b, c, d, e, f, and g are molar fractions, and 6≦a≦20, 3≦b≦12, 20≦c≦30, 32≦d≦45, 0≦e≦12, 0.01≦f≦1, and 0.05≦g≦1.5. The preparing methods comprises the following steps: 1) selecting source compounds of above elements; 2) mixing and grinding the source compounds to obtain a mixture; 3) presintering the mixture, then grinding the mixture; 4) sintering under reducing atmosphere, and cooling, thereby obtaining the luminescent material.
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机译:提供一种发光材料及其制备方法。硼硅酸盐发光材料的化学分子式为aM 2 Sub> O.bLn 2 Sub> O 3 Sub> .cAl 2 Sub> O < Sub> 3 Sub> .dR 2 Sub> O 3 Sub> .eSiO 2 Sub> .fCeO 2 Sub> .gTb 2 Sub> O 3 Sub>或aMO.bLn 2 Sub> O 3 Sub> .cAl 2 Sub> O 3 Sub> .dR 2 Sub> O 3 Sub> .eSiO 2 Sub> .fCeO 2 Sub> .gTb 2 Sub> O 3 Sub>,其中M为碱土金属或碱金属,Ln为选自元素Y和Gd的一种或两种元素; R是选自元素B和P的一个或两个元素; a,b,c,d,e,f和g为摩尔分数,且6≤a≤20、3≤b≤12、20≤c≤30、32≤d≤45、0≤e≤12、0.01 ≤f≤1,并且0.05≤g≤1.5。该制备方法包括以下步骤:1)选择上述元素的来源化合物; 2)将原料化合物混合并研磨以获得混合物; 3)预烧结混合物,然后研磨混合物; 4)在还原气氛下烧结,并冷却,从而获得发光材料。
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