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Method for preparation of carbon electrode, the carbon electrode obtained by this method and its application for the determination of thiocholine

机译:碳电极的制备方法,所得碳电极及其在硫代胆碱测定中的应用

摘要

the subject of the invention is how to prepare the carbon electrodes covering the substrate elektrodowy, consisting of at least two stages where the first stage is elektroforezu0119 includes: (a) placing the substrate elektrodowego and przeciwelektrody in vessel containing zawies ina carbon nanoparticles, cnps in solvent(b) a tension between the substrate elektrodowy and przeciwelektrodu0119, (c) the flow of charged particles from the solution to the substrate elektrodowego and second stage includes: (a) combining particles in aggregates, (b) deposition on the surface of the substrate elektrodowego formed aggregates, c) formation of film on the surface of the substrate elektrodowego homologous with that,the solvent is acetonitrile and based particles are exclusively carbon nanoparticles, cnps, favourably modified negatively charged polaric fenylosulfonowymi groups.disclosed is also obtained in this way with a carbon electrode that consists of a substrate elektrodowego and embedded directly on carbon nanoparticles, cnps, favourably modified negatively charged polaric groups fenylosulfonowymi and apply this carbon electrodes for the determination of tiocholiny.
机译:本发明的主题是如何制备覆盖基底电电极的碳电极,该碳电极包括至少两个阶段,其中第一阶段是电电极,包括:(a)将基底电电极和przeciwelektrody放置在碳纳米颗粒中的含有锯齿的容器中,溶剂中的cnps(b)基质电和przeciwelektrod之间的张力,(c)带电粒子从溶液流到基质电,第二阶段包括:(a)结合颗粒成团,(b)沉积在底物的表面形成聚集体,c)与底物表面同源的膜形成,溶剂是乙腈,基体颗粒仅是碳纳米粒子,碳纳米管,有利地修饰的带负电的极性联苯磺酰基基团。用碳电极以这种方式获得,该碳电极由基质elektrodowego和嵌入式二氧化钛组成在碳纳米粒子cnps上直接修饰,修饰成带负电荷的极性基团fenylosulfonowymi,并将该碳电极用于测定噻唑啉。

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