首页> 外国专利> METHOD FOR LIPOIC ACID MEASUREMENT IN BIOLOGICALLY ACTIVE ADDITIVES BY CATHODE VOLTAMMETRY

METHOD FOR LIPOIC ACID MEASUREMENT IN BIOLOGICALLY ACTIVE ADDITIVES BY CATHODE VOLTAMMETRY

机译:阴极伏安法测定生物活性添加剂中脂酸的方法。

摘要

FIELD: medicine.;SUBSTANCE: invention describes a method for lipoic acid measurement in biologically active additives by cathode voltammetry involving transferring a substance from a sample into a solution and taking voltammetric measurement; the cathode voltammetry is performed on a mercury-film electrode at potential -0.373 V of a relatively saturated silver-chloride electrode with borate buffer solution pH 9.18 at continuously current potential trace at 0.06 V/s with the determined lipoic acid content range from 4.5·106 to 1.1·10-3 mole/l.;EFFECT: improving sensitivity and expressivity of the method for measuring lipoic acid in tabletted BAAs by cathode voltammetry.;1 tbl, 1 ex, 3 dwg
机译:发明领域本发明描述了一种通过阴极伏安法测量生物活性添加剂中硫辛酸的方法,该方法包括将物质从样品转移到溶液中并进行伏安法测量。阴极伏安法是在相对饱和的氯化银电极,硼酸缓冲溶液pH为9.18,电势为0.06 V / s,连续电流为0.06 V / s的条件下,在汞膜电极上以-0.373 V的电势进行的,其硫辛酸含量范围为4.5· 10 6 至1.1·10 -3 摩尔/升;效果:提高了阴极伏安法测定压片BAA中硫辛酸的方法的灵敏度和表达能力; 1 tbl ,1前,3 dwg

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