首页> 外国专利> METHOD FOR TREATING DRAIN CONTAINING SULFUR-CONTAINING COMPOUND GENERATED IN MANUFACTURING PROCESS OF POLYARYLENE SULFIDE AND MANUFACTURING METHOD OF POLYARYLENE SULFIDE

METHOD FOR TREATING DRAIN CONTAINING SULFUR-CONTAINING COMPOUND GENERATED IN MANUFACTURING PROCESS OF POLYARYLENE SULFIDE AND MANUFACTURING METHOD OF POLYARYLENE SULFIDE

机译:聚硫醚制造过程中产生的含硫化合物的处理方法及聚硫醚的制造方法

摘要

PROBLEM TO BE SOLVED: To provide a method of treating drain capable of reducing percentage content of sulfide ion (S) and further COD material or BOD material efficiently and economically for drain generated in manufacturing polyarylene sulfide (PAS) in a predetermined range and reducing environmental load, and a manufacturing method of PAS making recovery and recycling a resin component in the drain easy.SOLUTION: There are provided a method of treating drain containing a sulfur-containing compound generated in a manufacturing process of PAS, which reduces Sconcentration in the drain after the treatment to 30 mg/L or less, preferably further COD material concentration to 3500 mg/L and/or BOD material concentration to 2500 mg/L or less by including a process of a wet oxidation treatment process of drain generated in a manufacturing process of PAS by polymerization reacting a sulfur source and dihaloaromatic compound in a solar organic solvent with heating, containing the sulfur-containing compound and mainly containing water under a condition of temperature of 130 to 320°C and pressure of 0.3 to 20 MPa, especially under alkali condition and further a solid liquid separation process and the manufacturing method of PAS.SELECTED DRAWING: None
机译:解决的问题:提供一种处理排水的方法,该方法能够在预定范围内有效降低生产制造聚亚芳基硫(PAS)中所产生的废水中的硫化物离子(S)和其他COD材料或BOD材料的百分比,并降低经济性。解决方案:提供了一种处理包含在PAS制造过程中产生的含硫化合物的排水装置的方法,该方法可减少排水装置中的S浓度。处理后,通过包括制造中产生的排出物的湿式氧化处理工序,优选进一步将COD材料浓度提高至3500mg / L和/或将BOD材料浓度降低至2500mg / L以下。硫源和二卤代芳族化合物在太阳能有机溶剂中加热加热聚合反应而制得的PAS的方法尤其是在碱性条件下,在130至320°C的温度和0.3至20 MPa的压力下主要包含水的化合物,以及进一步的固液分离工艺和PAS的制造方法。

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