首页> 外国专利> METHOD OF PRODUCTION OF A MATERIAL WITH PHOTOCATALYTIC AND BIOCIDAL PROPERTIES CONTAINING SPATIALLY ORIENTED TITANIUM DIOXIDE NANOTUBES MODIFIED WITH METALS PARTICULARLY PRECIOUS METALS

METHOD OF PRODUCTION OF A MATERIAL WITH PHOTOCATALYTIC AND BIOCIDAL PROPERTIES CONTAINING SPATIALLY ORIENTED TITANIUM DIOXIDE NANOTUBES MODIFIED WITH METALS PARTICULARLY PRECIOUS METALS

机译:一种具有光催化和生物杀菌特性的材料的制造方法,该材料包含空间定向的二氧化钛纳米管,并用金属特别是贵金属进行了改性

摘要

Method of production of a material with photocatalytic and biocidal properties containing spatially oriented titanium dioxide nanotubes modified with metals particularly precious metals. The method of production of a material with photocatalytic and biocidal properties containing spatially oriented titanium dioxide nanotubes modified with metals particularly precious metals consisting in being subjected to induced electric current placed in an electrolyte containing ammonium fluoride and ethylene glycol of the base containing titanium preferably titanium foil cleaning the obtained material with ultrasounds and then drying and calcinating is characterised according to the invention by the fact that the received material is placed in a multi component solution preferably in the neutral gas atmosphere. A multi component solution must contain 30 50% of alcohol by weight preferably isopropanol as well as ions and/or nanomolecules of one or several metals preferably two or three selected from the groups including silver gold platinum palladium ruthenium copper zinc nickel rhodium tungsten cobalt iron in the amount of 0.05 5% of the weight each as well as water. The mutual weight ratio of the metals is determined to be between 1: 1 and 1: 10. Preferably the multi component solution is mixed in darkroom conditions for 3 180 min preferably 120 min. Next it is irradiated with an UV emitting lamps for 0.5 6 hrs dried at the temperature of 60 100° C for 0.5 24 hrs favourably for 6 12 hrs.
机译:具有光催化和杀生物特性的材料的生产方法,该材料包含用金属特别是贵金属改性的空间取向的二氧化钛纳米管。一种具有光催化和杀生物特性的材料的制造方法,该材料包含空间取向的二氧化钛纳米管,该纳米管用金属特别是贵金属改性,该纳米二氧化钛纳米管受到感应电流的影响,该电流置于含有钛的基底的,优选为钛箔的含有氟化铵和乙二醇的电解质中根据本发明的特征在于,用超声波清洗所获得的材料,然后干燥并煅烧,其特征在于,将所接收的材料置于多组分溶液中,优选在中性气体气氛中。多组分溶液必须包含30 50%重量比的醇,优选异丙醇,以及一种或多种金属的离子和/或纳米分子,优选选自银,金,铂,钯,钌,铜,锌,镍,铑,钨,钴,铁等金属中的一种或几种。每份重量的0.05%以及水。确定金属的相互重量比在1:1和1:10之间。优选地,将多组分溶液在暗室条件下混合3180分钟,优选120分钟。接下来,用UV发射灯照射0.5×6小时,在60100℃的温度下干燥0.5×24小时,优选6×12小时。

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