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Method for producing CdSe/ZnS/PVP nanocomposite

机译:CdSe / ZnS / PVP纳米复合材料的制备方法

摘要

The invention relates to nanotechnology, particularly to methods for producing nanocomposite layers, and can be used in medicine and optoelectronics.The method for producing CdSe/ZnS/PVP nanocomposite comprises the separate preparation of the colloidal solution of nanoparticles or CdSe/ZnS nanosuspension and polyvinylpyrrolidone solution using hydrophilic solvents: acetone, acetylacetone, mixing thereof, wherein the ratio of CdSe/ZnS and polyvinylpyrrolidone is equal to 1…10, dispersion of the resulting mixture in an ultrasonic bath for 5…30 min, placement of the dispersed mixture, for electrophoretic deposition, in a cell with two electrodes, placed at a distance of 10 mm from one another, one of which is made of glass and coated with In2O3-SnO2 (1TO), and the second - of titanium, supply of electrodes with constant voltage of 700 V for 3…30 min up to the formation of a film nanocomposite on the glass electrode.
机译:本发明涉及纳米技术,尤其涉及纳米复合层的制备方法,可用于医药和光电领域。制备CdSe / ZnS / PVP纳米复合材料的方法包括分别制备纳米胶体溶液或CdSe / ZnS纳米悬浮体和聚乙烯吡咯烷酮。使用亲水性溶剂的溶液:丙酮,乙酰丙酮,其混合,其中CdSe / ZnS和聚乙烯吡咯烷酮之比等于1…10,将所得混合物在超声浴中分散5…30分钟,将分散的混合物放置在在具有两个电极的电池中进行电泳沉积,两个电极之间的距离为10 mm,其中一个由玻璃制成并涂有In2O3-SnO2(1TO)涂层,第二个由钛制成,电极供应恒定700 V电压持续3…30分钟,直到在玻璃电极上形成薄膜纳米复合材料。

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