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COMPOSITE MATERIAL BASED ON SIO2 MATRIX METHOD AND ITS RECEIPT

机译:基于SIO2矩阵方法的复合材料及其接收

摘要

The invention relates to manufacturing technology scintillation detectors for registration of ionizing radiation for medical diagnostic equipment, custom systems, dosimetric and spectrometric devices. Composite materials based on SiO2 matrix consisting of an optical medium, which is SiO2 matrix, and activator-organic scintillator, which is the phosphor 1,2-bis (5-phenyl-2-oxazolyl) -benzolu (o-ROROR) or 2 5 dyfeniloksazolu (PPO), and the activator content is 3-5 wt. %. Also proposed method of composite material based on SiO2 matrix comprising solution for SiO2 matrix with a volume ratio of components tetrametoksysylan: methanol: water: monobasic inorganic acid is 1: 0.84: 1.2: 0.14, respectively, while stirring, transfusion resulting solution in sealed containers to hold the gel formation and drying it in the formation of the matrix, additional annealing the resulting matrix, the matrix impregnated within 24-48 hours. organic phosphor solution of 1,2-bis (5-phenyl-2-oxazolyl) -benzolu (o-ROROR) or 2.5 dyfeniloksazolu (PPO) in an organic solvent, concentration of the phosphor in a solvent 5-10 wt. %, Drying the resulting composite scintillator at a temperature of 40-50 ° C to mass constancy. Manufacturing of composite material that is claimed, does not require additional cleaning costs for raw materials, the use of the value of the growth equipment.
机译:本发明涉及用于医疗诊断设备,定制系统,剂量和光谱测定设备的电离辐射配准的闪烁探测器的制造技术。基于SiO2基质的复合材料,该复合材料由一种光学介质(即SiO2基质)和一种活化剂-有机闪烁体(一种荧光粉1,2-双(5-苯基-2-恶唑基)-苯并(o-ROROR)或2)组成5 dyfeniloksazolu(PPO),活化剂含量为3-5 wt。 %。还提出了一种基于SiO2基体的复合材料的方法,该方法包括用于SiO2基体的溶液,其组分的比例为四甲吡喃:甲醇:水:一元无机酸分别为1:0.84:1.2:0.14,同时搅拌,将所得溶液输注到密封容器中为了保持凝胶的形成并使其在基质的形成中干燥,对所得基质进行额外的退火处理,基质在24-48小时内浸渍。在有机溶剂中的1,2-双(5-苯基-2-恶唑基)-苯并(o-ROROR)或2.5二氟代偶氮唑(PPO)的有机磷光体溶液,磷光体在溶剂中的浓度为5-10 wt。 %,在40-50℃的温度下干燥所得复合闪烁体至质量恒定。要求保护的复合材料的制造不需要原材料的额外清洁成本,无需使用生长设备的价值。

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