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METHOD FOR EXTRACTING CHLOROGENIC ACID FROM EUCOMMIA LEAVES

机译:从杜仲叶中提取绿原酸的方法

摘要

Provided is a method for extracting chlorogenic acid from Eucommia leaves, comprising the following steps: a, weighing of Eucommia leaves; b, water extraction; c, pre-treatment; d, filtration; e, loading on a macroporous adsorbent resin; f, concentrating; g, drying: spray drying, an air inlet temperature being 150oC - 200oC, and an air outlet temperature being 50oC - 90oC, thereby obtaining a chlorogenic acid crude product. The present invention uses water extraction, pre-treatment, loading on a macroporous adsorbent resin column, concentrating and drying to prepare the chlorogenic acid crude product. A water extract liquid is not concentrated, and is directly loaded on the macroporous adsorbent resin for purification treatment after being pre-treated, thereby solving the problem of decomposition caused by chlorogenic acid being concentrated in water for a long time and heated unstably, at the same time as omitting a concentrating process link to shorten the production cycle. In addition, a crude product having 20-60% of various specifications may be produced by controlling concentration parameters of different eluents.
机译:提供一种从杜仲叶中提取绿原酸的方法,包括以下步骤:a,称量杜仲叶的重量; b,水提取; c,预处理; d,过滤; e,加载到大孔吸附树脂上; f,专心; g,干燥:喷雾干燥,进风温度为150 o C-200 o C,出风温度为50 o C -90℃,由此获得绿原酸粗产物。本发明使用水提取,预处理,将其装载在大孔吸附树脂柱上,浓缩并干燥以制备绿原酸粗产物。提取液不浓缩,经预处理后直接负载在大孔吸附树脂上进行纯化处理,从而解决了绿原酸长时间在水中浓缩并不稳定加热引起的分解问题。同时省去了浓缩工艺环节,以缩短生产周期。此外,可以通过控制不同洗脱液的浓度参数来生产具有20-60%各种规格的粗产物。

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