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METHOD FOR EXTRACTING CHLOROGENIC ACID FROM EUCOMMIA LEAVES

机译:从杜仲叶中提取绿原酸的方法

摘要

The present invention provides a kind of methods from extracting chlorogenic acid from Eucommia leaves, it includes the following steps: a, weighs folium cortex eucommiae; B, water extracts; C, it pre-processes; D, it filters; E, upper macroporous absorbent resin; F, it is concentrated; G, drying: spray drying: 150 DEG C -200 DEG C of intake air temperature, 50 DEG C -90 DEG C of air outlet temperature to get chlorogenic acid crude product. The present invention is mentioned using water, is pre-processed, upper large pore resin absorption column, is concentrated and dried to prepare chlorogenic acid crude product. Aqueous extract is not concentrated and directly upper macroporous absorbent resin carries out purification process after pre-processing, and solves the problems, such as that chlorogenic acid is led to decomposition by thermally labile for a long time in water because being concentrated, while saving enrichment process link and shortening the production cycle. In addition, the crude product of 20-60% various specifications can be produced by controlling the concentration parameter of different eluents.
机译:本发明提供了一种从杜仲叶中提取绿原酸的方法,包括以下步骤:a,称量杜仲叶; B,水提物; C,预处理; D,过滤器; E,上部大孔吸收性树脂; F,它是集中的; G,干燥:喷雾干燥:进风温度为150℃-200℃,出风温度为50℃-90℃,得到绿原酸粗产物。提到本发明时使用水,对其进行预处理,上部是大孔树脂吸收塔,浓缩并干燥以制备绿原酸粗产物。水提取物不浓缩,直接在上层大孔吸收性树脂预处理后进行纯化处理,解决了绿原酸由于浓缩而在水中长时间热不稳定导致绿原酸分解的问题,同时节省了浓缩工艺环节,缩短生产周期。此外,通过控制不同洗脱液的浓度参数,可以生产出各种规格的20-60%的粗产物。

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