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THERMAL SEPARATION OF SOLUTION COMPOSED BY THERMOPLASTIC POLYMER AND SOLVENT

机译:热塑聚合物和溶剂组成的溶液的热分离

摘要

FIELD: process engineering.;SUBSTANCE: invention relates to thermal separation of solution composed by thermoplastic polymer and solvent. This solution is heated at overpressure to above the solvent critical point and, then, decompressed in high pressure separator. Note here that formed are the phase with high content of polymer and the phase with low content of polymer. The former is fed into the mixer. Pressure difference at the mixer inlet causes the instant thermal evaporation in the mixer to make the heavy phase polymer increase to at least 70%. Obtained solution with high content of polymer is fed, particularly, that distributed, at least partially, along the mixer shaft length part. Said mixer is located inside said space to heat the polymer bulk by the energy of mechanical mixing. This ups the polymer portion to above 70%.;EFFECT: higher molecular mass, decreased amount of fine particles, higher efficiency, lower residual content of unwanted volatile substances, electric power saving.;6 cl, 2 dwg, 1 tbl
机译:技术领域本发明涉及由热塑性聚合物和溶剂组成的溶液的热分离。将该溶液在超压下加热到溶剂临界点以上,然后在高压分离器中减压。在此注意,形成的是具有高聚合物含量的相和具有低聚合物含量的相。前者被送入混合器。混合器入口处的压差导致混合器中的瞬时热蒸发,使重相聚合物增加到至少70%。所获得的具有高聚合物含量的溶液尤其是沿混合器轴长度部分至少部分地分配的溶液被进料。所述混合器位于所述空间内,以通过机械混合的能量加热聚合物本体。这将聚合物部分提高到70%以上。效果:更高的分子量,减少的细颗粒数量,更高的效率,更低的不想要的挥发性物质残留量,节省了电能; 6 cl,2 dwg,1 tbl

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