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METHOD OF REMOVING ORGANIC AND INORGANIC ACIDS FROM REACTION MASS OF DECOMPOSITION OF ISOPROPYL BENZENE HYDROPEROXIDE

机译:从异丙基苯过氧化氢分解反应中脱除有机酸和无机酸的方法

摘要

FIELD: chemistry.;SUBSTANCE: neutralisation of acids is carried out in two steps: the first step includes primary neutralisation of acids, primarily sulphuric acid, on an assembly consisting of three filters with a fixed anion-exchange resin layer, said filters operating on a "carousel" scheme, wherein neutralisation of acids is carried out on two series-connected filters, a third filter being regenerated at that time; at the second step the acid remaining in the decomposition reaction mass is neutralised with aqueous alkali solution.;EFFECT: reduced content of salts in the decomposition reaction mass before fractionation thereof and therefore reduced amount of salts in the phenol resin, high output and improved quality of the end product.;1 dwg, 4 tbl, 3 ex
机译:领域:化学;物质:酸的中和分两个步骤进行:第一步包括在由三个带有固定阴离子交换树脂层的过滤器组成的组件上对酸(主要是硫酸)进行初步中和,所述过滤器在一种“旋转木马”方案,其中酸的中和是在两个串联的过滤器上进行的,此时第三个过滤器被再生;在第二步中,用碱水溶液中和分解反应物料中残留的酸。效果:分解反应物料中的盐含量降低,然后分馏,从而减少了酚醛树脂中的盐量,提高了产量,提高了质量最终产品的数量。; 1 dwg,4 tbl,3 ex

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