首页> 外国专利> THE METHOD OF ISOLATION AND PURIFICATION OF (MONO- AND DI-SUBSTITUTED) CHITIN ESTERS AND CHITIN COPOLYESTERS FROM REACTION MIXTURES

THE METHOD OF ISOLATION AND PURIFICATION OF (MONO- AND DI-SUBSTITUTED) CHITIN ESTERS AND CHITIN COPOLYESTERS FROM REACTION MIXTURES

机译:从反应混合物中分离和纯化(单和二取代的)几丁质酯和几丁质共聚酯的方法

摘要

The invention consists in the method of isolation and purification of mono- and/or di- substituted esters and copolyesters of chitin from reaction mixtures. The method is based on adding to the reaction mixture containing the products of chitin acylation performed using the acid anhydrides in the presence of respective catalysts with aqueous solution of acidic sodium carbonate and subsequent grinding of the reaction mixture in order to obtain a homogeneous precipitate, which is then washed by solvent, dried and dissolved in solvent, precipitated in water and finally washed again by water.
机译:本发明在于从反应混合物中分离和纯化几丁质的单和/或二取代的酯和共聚酯的方法。该方法是基于在含有催化剂的反应混合物中加入使用酸酐在酸性碳酸钠水溶液中使用酸酐进行的几丁质酰化产物,然后将反应混合物研磨以获得均匀的沉淀,然后用溶剂洗涤,干燥并溶于溶剂,在水中沉淀,最后再次用水洗涤。

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