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HYDROGEN STORAGE CAPACITY MEASUREMENT METHOD AND HYDROGEN STORAGE CAPACITY MEASUREMENT APPARATUS

机译:氢存储容量的测定方法及氢存储容量的测定装置

摘要

PROBLEM TO BE SOLVED: To provide a hydrogen storage capacity measurement method which allows measurement even under a mixture gas atmosphere.SOLUTION: First of all, in the state at prescribed temperature in a vacuum, a sample 3 is irradiated with X-rays to acquire X-ray diffraction data (step S1). Next, in the state at prescribed temperature with prescribed pressure under an atmosphere of hydrogen or mixture gas containing hydrogen, the sample 3 is irradiated with X-rays to acquire X-ray diffraction data (step S2). Next, a lattice volume is calculated using the X-ray diffraction data acquired in the steps S1 and S2 to calculate a lattice volume expansion amount (step S3). Next, using a relation between a lattice volume expansion amount corresponding to crystal structure of the sample 3 and hydrogen storage capacity, hydrogen storage capacity is calculated from the lattice volume expansion amount calculated in the step S2 (step S4).SELECTED DRAWING: Figure 4
机译:要解决的问题:提供一种即使在混合气体气氛下也能进行测量的储氢容量测量方法。解决方案:首先,在规定温度的真空状态下,对样品3进行X射线辐照以获取X射线衍射数据(步骤S1)。接着,在氢气或含有氢气的混合气体的气氛中,在规定温度,规定压力的状态下,对试样3照射X射线,取得X射线衍射数据(步骤S2)。接下来,使用在步骤S1和S2中获取的X射线衍射数据计算晶格体积,以计算晶格体积膨胀量(步骤S3)。接下来,利用与样品3的晶体结构相对应的晶格体积膨胀量与储氢容量之间的关系,由在步骤S2中计算出的晶格体积膨胀量来计算储氢容量(步骤S4)。图4:

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