首页> 外国专利> ORGANOTIN CONTAINING HYPERBRANCHED POLYSILOXANE STRUCTURE AND PREPARATION METHOD THEREFOR

ORGANOTIN CONTAINING HYPERBRANCHED POLYSILOXANE STRUCTURE AND PREPARATION METHOD THEREFOR

机译:含有机锡的超支化聚硅氧烷结构及其制备方法

摘要

A method of preparing an organotin containing hyperbranched polysiloxane structure includes the following steps: (1) by weight, 0.5-1.5 portions of hyperbranched polysiloxane with reactive functional groups is dissolved in 50-100 portions of an alcohol solvent, to obtain a solution A; (2) by weight, 0.5-0.9 portions of a tin-based initiator and 50-100 portions of the alcohol solvent are mixed to obtain a solution B, wherein said tin-based initiator is selected from dihydroxy butyl tin chloride, butyl tin trichloride, and dibutyl tin dichloride; and (3) dropping the solution B into the solution A at the temperature of 0° C.-60° C., reacting for 3-6 h, filtering and drying to obtain the organotin containing hyperbranched polysiloxane structure.
机译:一种含有机锡的超支化聚硅氧烷结构的制备方法,包括以下步骤:(1)将0.5-1.5重量份的具有反应性官能团的超支化聚硅氧烷溶解在50-100份的醇溶剂中,得到溶液A; (2)按重量计,将0.5-0.9份锡基引发剂和50-100份醇溶剂混合以获得溶液B,其中所述锡基引发剂选自二羟基丁基氯化锡,三氯化丁基锡。和二丁基二氯化锡; (3)在0℃-60℃的温度下将溶液B滴入溶液A中,反应3-6小时,过滤并干燥,得到含有机锡的超支化聚硅氧烷结构。

著录项

  • 公开/公告号US2017204228A1

    专利类型

  • 公开/公告日2017-07-20

    原文格式PDF

  • 申请/专利权人 SOOCHOW UNIVERISTY;

    申请/专利号US201515328008

  • 申请日2015-05-28

  • 分类号C08G79/12;C08G77/26;C08G77/18;C08G77/398;

  • 国家 US

  • 入库时间 2022-08-21 13:52:15

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