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Manufacturing method of metal catalyst-supporting carrier, metal catalyst-supporting carrier, manufacturing method of fuel cell and catalyst supporting device

机译:金属催化剂担载载体的制造方法,金属催化剂担载载体,燃料电池的制造方法和催化剂担载装置

摘要

There is provided a technique that suppresses a variation in particle diameter of a metal catalyst in the process of supporting the metal catalyst on a carrier. A CNT substrate having carbon nanotubes (CNTs) as the carrier arrayed thereon is placed in a processing chamber. Carbon dioxide is supplied to the processing chamber. After the carbon dioxide in the processing chamber is made supercritical, a complex solution in which a platinum complex is dissolved is supplied to the processing chamber. A sample temperature denoting temperature of the CNTs is controlled to be higher than an ambient temperature in the processing chamber. The CNT substrate is heated, such that a temperature difference between the ambient temperature and the sample temperature repeats increasing and decreasing. After the state of the supercritical fluid is changed to a non-supercritical state, the CNT substrate is heated, so as to cause the metal catalyst to deposit on the surface of the CNTs.
机译:提供了一种在将金属催化剂负载在载体上的过程中抑制金属催化剂的粒径变化的技术。将具有碳纳米管(CNT)作为其上排列的载体的CNT基板放置在处理室中。二氧化碳被供应到处理室。在使处理室中的二氧化碳超临界之后,将溶解有铂络合物的络合物溶液供应至处理室。表示CNT的温度的样品温度被控制为高于处理室中的环境温度。加热CNT衬底,使得环境温度和样品温度之间的温度差重复增加和减少。在超临界流体的状态变为非超临界状态后,加热CNT基板,以使金属催化剂沉积在CNT的表面上。

著录项

  • 公开/公告号US9692059B2

    专利类型

  • 公开/公告日2017-06-27

    原文格式PDF

  • 申请/专利权人 TOYOTA JIDOSHA KABUSHIKI KAISHA;

    申请/专利号US201214646082

  • 发明设计人 RYOICHI NANBA;

    申请日2012-11-21

  • 分类号B01J23/58;B01J23/63;H01M4/90;H01M4/88;B01J21/18;B01J23/56;B01J23/70;H01M4/92;H01M8/1018;

  • 国家 US

  • 入库时间 2022-08-21 13:43:11

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