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DICYCLOPENTADIENE COMPOUND-MODIFIED PHENOLIC RESIN PRODUCTION METHOD

机译:双环戊二烯复合改性酚醛树脂的生产方法

摘要

The purpose of the present invention is to provide a dicyclopentadiene compound-modified phenolic resin production method, whereby, when a catalyst is used repeatedly in the method, it becomes possible to stabilize the properties and color of the resin and it also becomes possible to use the catalyst repeatedly a sufficient number of times. The present invention addresses the problem of providing: a dicyclopentadiene compound-modified phenolic resin production method for producing a dicyclopentadiene compound-modified phenolic resin by reacting a phenol compound with a dicyclopentadiene compound, wherein a fluorinated ion exchange resin, which is used as a catalyst in the production, is re-used as a catalyst for the reaction between the phenol compound and the dicyclopentadiene compound to produce the dicyclopentadiene compound-modified phenolic resin, said method being characterized in that the fluorinated ion exchange resin to be re-used is washed with an organic solvent and the washed fluorinated ion exchange resin is used at least once during the re-use of the fluorinated ion exchange resin; and a production method as mentioned above, which is employed for purifying the product and whereby it becomes possible to prevent the discoloration of the resin produced in the above-mentioned dicyclopentadiene compound-modified phenolic resin production. The dicyclopentadiene compound-modified phenolic resin produced by the production method according to the present invention has stable quality and high purity and is inexpensive.
机译:本发明的目的是提供一种二环戊二烯化合物改性的酚醛树脂的生产方法,由此,当在该方法中重复使用催化剂时,可以稳定树脂的性质和颜色,并且也可以使用催化剂重复多次。本发明解决了提供以下问题:提供一种通过使酚化合物与二环戊二烯化合物反应来生产二环戊二烯化合物改性的酚醛树脂的二环戊二烯化合物改性的酚醛树脂的方法,其中氟化的离子交换树脂用作催化剂。在生产过程中,将其再用作酚化合物与二环戊二烯化合物之间反应以生产二环戊二烯化合物改性酚醛树脂的催化剂,所述方法的特征在于,洗涤要再利用的氟化离子交换树脂与有机溶剂一起使用,并且在氟离子交换树脂的再使用期间,至少将洗涤过的氟离子交换树脂使用一次。以及如上所述的生产方法,其用于纯化产物,从而可以防止在上述二环戊二烯化合物改性的酚醛树脂生产中生产的树脂的变色。通过根据本发明的生产方法生产的二环戊二烯化合物改性的酚醛树脂具有稳定的质量和高纯度并且便宜。

著录项

  • 公开/公告号WO2017026099A1

    专利类型

  • 公开/公告日2017-02-16

    原文格式PDF

  • 申请/专利权人 JFE CHEMICAL CORPORATION;

    申请/专利号WO2016JP03488

  • 发明设计人 TAKEMURA KAZUYA;

    申请日2016-07-28

  • 分类号C08G61/02;

  • 国家 WO

  • 入库时间 2022-08-21 13:32:12

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