首页> 外国专利> METHOD OF MANUFACTURING QUANTUM DOT USING METAL OXIDE NANOPARTICLE WITH HIGH SPECIFIC SURFACE AREA AND QUANTUM DOT MANUFACTURED BY THE METHOD

METHOD OF MANUFACTURING QUANTUM DOT USING METAL OXIDE NANOPARTICLE WITH HIGH SPECIFIC SURFACE AREA AND QUANTUM DOT MANUFACTURED BY THE METHOD

机译:利用具有高比表面积的金属氧化物纳米粒子制造量子点的方法及由该方法制造的量子点

摘要

The present invention relates to a method of preparing a quantum dot with excellent thermal stability and light-scattering properties using nano-metal oxides. The purpose of the present invention is to provide a method of preparing a quantum dot which can be dispersed in various polar solvents by synthesizing particles which are excellent in thermal stability, light-scattering properties and dispersion stability, and may have hydrophilic and hydrophobic characteristics. To this end, the present invention provides the method of preparing the quantum dot, and the quantum dot prepared by the method, the method comprises the steps of: (a) mixing at least one selected from zinc (Zn), cadmium (Cd), indium (In) and copper (Cu) with an unsaturated fatty acid, and adding an ethylene-based hydrocarbon organic solvent to the mixture to synthesize a cationic precursor; (b) mixing at least one among selenium (Se), sulfur (S), phosphorous (P) and tellurium (Te) with any one series group selected from alkylphosphine series, alkylphosphine oxide series and trialkylphosphine series to synthesize an anionic precursor; and (c) mixing the cationic precursor synthesized in the step (a) with the anionic precursor synthesized in the step (b) at a predetermined ratio, and making the cationic precursor synthesized in the step (a) react with the anionic precursor synthesized in the step (b) at a predetermined temperature to synthesize the quantum dot.
机译:本发明涉及一种使用纳米金属氧化物制备具有优异的热稳定性和光散射特性的量子点的方法。本发明的目的是提供一种制备量子点的方法,该量子点可以通过合成具有优异的热稳定性,光散射性质和分散稳定性并且可以具有亲水和疏水特性的颗粒而分散在各种极性溶剂中。为此,本发明提供了制备量子点的方法,以及通过该方法制备的量子点,该方法包括以下步骤:(a)混合选自锌(Zn),镉(Cd)中的至少一种。 ,铟(In)和铜(Cu)与不饱和脂肪酸的混合物,并向该混合物中加入基于乙烯的烃类有机溶剂以合成阳离子前体; (b)将硒(Se),硫(S),磷(P)和碲(Te)中的至少一种与选自烷基膦系列,烷基氧化膦系列和三烷基膦系列中的任何一个系列基团混合以合成阴离子前体; (c)将步骤(a)中合成的阳离子前体与步骤(b)中合成的阴离子前体以预定比例混合,并使步骤(a)中合成的阳离子前体与在步骤(b)中合成的阴离子前体反应。在预定温度下进行步骤(b)以合成量子点。

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