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METHOD OF CONTROLLED CHEMICAL INTERACTIONS surface of solid fillers and additives to produce a product FILLER SURFACED

机译:固体填料和添加剂的化学相互作用表面控制方法,用于生产填充表面的产品

摘要

1. A process for preparing a filler product surfaced with succinic (bubbled) anhydride (s), wherein the method comprises at least the steps of: a) providing at least one filler comprising calcium carbonate, imeyuschegoi) a weight average particle size d in the range from 0.1 .mu.m to 7 .mu.m, ii) an upper limit value (d) ≤15 microns, iii) a specific surface area (BET) of from 0.5 to 150 m / g as determined by the nitrogen BET method, and iv) residual total moisture content from 0.01 to 1 wt.%, based on the total dry weight of at least one material a filler comprising calcium carbonate, b) obtaining at least one mono-substituted succinic anhydride, and, optionally, at least one mono-substituted succinic acid in an amount of from 0.1 to 3 wt.%, based on the total dry weight of at least one filler comprising calcium carbonate material of step a), c) contacting the surface of at least one filler containing calcium carbonate of step a) with stirring, in one or more stages, at least with a mono-substituted Yantai nym anhydride and, optionally, at least one mono-substituted succinic acid with stadiib) so that the layer has been processed, comprising at least one mono-substituted succinic anhydride, and optionally at least one mono-substituted succinic acid and / or salt (s) product (s), their interaction is formed on the surface of said at least one filler containing calcium carbonate, in step a), wherein the temperature before and / or during the contacting step c) is adjusted so that evap and was at least 2 ° C above the melting temperature of
机译:1.一种制备用琥珀酸(鼓泡的)酸酐表面处理的填料产品的方法,其中所述方法至少包括以下步骤:a)提供至少一种包含碳酸钙的填料,以重量计,其粒径为d。范围从0.1微米至7微米,ii)上限值(d)≤15微米,iii)由氮确定的比表面积(BET)为0.5至150 m / g BET方法,以及iv)基于至少一种材料的总干重计,残留的总水分含量为0.01至1 wt。%,包括碳酸钙的填料,b)获得至少一种单取代的琥珀酸酐,以及可选的,基于至少一种包含步骤a)的碳酸钙材料的填充剂的总干重,至少一种单取代的琥珀酸的量为0.1至3重量%,c)接触至少一种的表面在一个或多个阶段中,至少在搅拌下,在步骤a)中包含步骤a)的碳酸钙的填料取代的烟台山姆酸酐和,任选地,至少一种单取代的琥珀酸与stadiib),使得该层已被处理,包含至少一种单取代的琥珀酸酐,以及任选的至少一种单取代的琥珀酸和在步骤a)中,在所述至少一种含碳酸钙的填料的表面上形成它们的相互作用,其中调节接触步骤c)之前和/或期间的温度,使得蒸发并且至少比熔融温度高2°C

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