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Electrochemical method for producing nanosized powders of holmium and nickel intermetallic compounds in halide melts

机译:卤化物熔体中制备nano和镍金属间化合物纳米级粉末的电化学方法

摘要

FIELD: chemistry.SUBSTANCE: invention relates to electrochemical production of holmium and nickel intermetallic compounds nanopowders, which can be used as catalysts in chemical and petrochemical industries, hydrogen energy for reversible sorption of hydrogen, as well as for magnetic material creation. Electrolysis of a molten mixture containing potassium chloride, sodium chloride, holmium (III) chloride and nickel (II) chloride is performed in a quartz cell on a tungsten electrode at a temperature of 973°K and a current density of 0.5÷1.9 A/cm.EFFECT: decreased temperature of electrolysis and obtaining of nickel and holmium intermetallic compounds nanopowders.6 dwg, 3 tbl, 5 ex
机译:electrochemical和镍金属间化合物纳米粉的电化学生产技术领域本发明涉及electrochemical和镍金属间化合物纳米粉的电化学生产,其可在化学和石油化学工业中用作催化剂,用于可逆吸附氢的氢能以及用于磁性材料的制造。含有氯化钾,氯化钠,氯化hol(III)和氯化镍(II)的熔融混合物的电解在石英电池中的钨电极上于973°K的温度下进行,电流密度为0.5÷1.9 A /效果:降低电解温度并获得镍和hol金属间化合物纳米粉体6 dwg,3 tbl,5 ex

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