FIELD: chemistry.;SUBSTANCE: invention relates to a method of producing molecular complex [1,2,5]oxadiazolo[3,4-e][1,2,3,4]-tetrazine-4,6-di-N-oxide with 2,4-dinitro-2,4-diazapentane (FTDO-DNP), involving preparation of a solution of [1,2,5]oxadiazolo[3,4-e][1,2,3,4]-tetrazine-4,6-di-N-oxide using a mixture of polar halogen-derivative aprotic solvents, adding to obtained solution 2,4-dinitro-2,4-diazapentane, mixing at a temperature of 11–15 °C, and then adding a non-polar hydrocarbon precipitator.;EFFECT: safe and efficient method of producing molecular complex FTDO-DNP which enables to increase output of end product.;3 cl, 6 ex
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机译:技术领域本发明涉及一种制备分子复合物[1,2,5]恶二唑[3,4-e] [1,2,3,4]-四嗪-4,6-di-N的方法2,4-二硝基-2,4-二氮杂戊烷(FTDO-DNP)氧化,涉及制备[1,2,5]恶二唑并[3,4-e] [1,2,3,4]的溶液-4-四嗪-4,6-二-N-氧化物,使用极性卤素衍生物非质子溶剂的混合物,添加到所得溶液2,4-二硝基-2,4-二氮戊烷中,在11–15°C的温度下混合,效果:安全有效的生产分子复合物FTDO-DNP的方法,可增加最终产物的产量。; 3 cl,6 ex
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