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Process for producing octachlorotrisilane and octachlorotrisilane produced by the process

机译:八氯三硅烷的生产方法和由该方法生产的八氯三硅烷

摘要

PROBLEM TO BE SOLVED: To provide a manufacturing method of octachlorotrisilane and to obtain octachlorotrisilane having a purity of 90 mass% or more by conducting the manufacturing method.SOLUTION: There is provided a manufacturing method including: a high temperature reaction process for reacting a raw material gas containing volatilized tetrachlorosilane and hydrogen at high temperature to obtain a reaction production gas containing trichlorosilane; an octachlorotrisilane production process for bringing the reaction production gas obtained by the high temperature reaction process into contact with a cooling liquid obtained by circulation cooling an aggregation liquid generated by cooling the reaction production gas and quickly cooling them to produce octachlorotrisilane in the aggregate liquid; and a recovery process for recovering the produced octachlorotrisilane.SELECTED DRAWING: Figure 1
机译:解决的问题:提供一种八氯三硅烷的制造方法,并通过进行该制造方法来获得纯度为90质量%以上的八氯三硅烷。解决方案:提供一种制造方法,包括:用于使原料反应的高温反应工艺。在高温下含有挥发的四氯硅烷和氢气的原料气,得到含有三氯硅烷的反应生成气。八氯三硅烷生产工艺,使通过高温反应工艺获得的反应生产气体与冷却液接触,该冷却液通过循环冷却由冷却反应生产气体产生的聚集液并快速冷却以在聚集液中生产八氯三硅烷而获得。以及用于回收生产的八氯三硅烷的回收方法。选图:图1

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