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Method for producing surface modified mesoporous silica nanoparticles

机译:表面改性的介孔二氧化硅纳米粒子的制备方法

摘要

PROBLEM TO BE SOLVED: To provide a modified mesoporous silica nanoparticle excellent in dispersibility in organic solvents and a method of producing a modified mesoporous silica nanoparticle which is excellent in dispersibility in organic solvents and has reactive groups on the surface of the nanoparticle.SOLUTION: A method of producing a mesoporous silica nanoparticle surface-modified with a silane coupling agent includes a step of preparing a mesoporous silica nanoparticle having a structure in which mesopores are arranged hexagonally and a step of mixing together, with stirring, a slurry prepared by wetting the mesoporous silica nanoparticle with an alcohol and a water/alcohol-based solution of a hydrolysate of a silane coupling obtained by adding an acid catalyst and modifying the surface of the mesoporous silica nanoparticle while being subjected to an ultrasonic treatment.
机译:解决的问题:提供一种在有机溶剂中具有优异分散性的改性介孔二氧化硅纳米粒子,以及一种制备在有机溶剂中具有优异分散性且在纳米粒子表面具有反应性基团的改性介孔二氧化硅纳米粒子的方法。生产用硅烷偶联剂表面改性的中孔二氧化硅纳米粒子的方法包括制备具有其中孔以六角形排列的结构的中孔二氧化硅纳米粒子的步骤,以及在搅拌下将通过润湿中孔制备的浆料混合在一起的步骤。通过在进行超声处理的同时添加酸催化剂并改性介孔二氧化硅纳米粒子的表面而获得的具有醇和硅烷偶联的水解产物的水/醇基溶液的二氧化硅纳米粒子。

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