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Method for correcting measurement error due to temperature displacement of measuring apparatus and mass spectrometer using the method

机译:用该方法校正由于测量装置和质谱仪的温度位移引起的测量误差的方法

摘要

A cylindrical rod-shaped reference member (5) made of a material having a coefficient of thermal expansion different from that of the flight tube (2) is placed in contact with the tube (2), and one end of the tube (2) and the reference member (5) is attached. Fix with the fixing part (6). The distance measuring sensor (7) measures the difference between the lengths of the tube (2) and the reference member (5) that fluctuate due to temperature changes. The displacement of this length difference is larger than the displacement of the length of the flight tube (2) itself in terms of the ratio. Further, the difference in length is much smaller than the length of the flight tube (2) itself. Therefore, the displacement due to thermal expansion can be captured with high accuracy while using an inexpensive sensor such as a strain gauge, and the m / z value of the mass spectrum data is corrected based on this measurement value. Mass deviation correction can be performed.
机译:由与膨胀管(2)具有不同的热膨胀系数的材料制成的圆柱形杆状基准构件(5)与该管(2)接触,并且该管(2)的一端接触。并且附接参考构件(5)。用固定部件(6)固定。距离测量传感器(7)测量由于温度变化而波动的管(2)和基准构件(5)的长度之差。就比率而言,该长度差的位移大于飞管(2)本身的长度的位移。此外,长度差远小于飞行管(2)本身的长度。因此,在使用廉价的传感器(例如应变仪)的同时,可以高精度地捕获由于热膨胀引起的位移,并且基于该测量值来校正质谱数据的m / z值。可以执行质量偏差校正。

著录项

  • 公开/公告号JPWO2017064802A1

    专利类型

  • 公开/公告日2018-05-24

    原文格式PDF

  • 申请/专利权人 株式会社島津製作所;

    申请/专利号JP20170545062

  • 发明设计人 山口 真一;

    申请日2015-10-16

  • 分类号G01N27/62;H01J49/40;

  • 国家 JP

  • 入库时间 2022-08-21 13:07:00

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