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Double-tilt in-situ mechanical sample holder for TEM based on piezoelectric ceramic drive

机译:基于压电陶瓷驱动的TEM双倾斜原位机械样品架

摘要

A double-tilt in-situ mechanical sample holder for TEM based on piezoelectric ceramic drive belongs to the field of material microstructure-mechanical properties in-situ characterization, and it comprise two parts of sample holder shaft body and piezoelectric ceramic drive system. The sample holder shaft body comprise tilt stage, sample holder, linear stepping motor, drive rod, drive linkage. The piezoelectric ceramic drive system comprise piezoelectric ceramic loading stage, piezoelectric ceramic, connecting base and the sample loading stage realizing stretch or compression function. The double-axis tilt of the samples in X and Y axis directions is realized by the reciprocating motion back and forth of the drive rod driven by the linear stepping motor. The stretch or compression of the samples is realized by applying voltage on the piezoelectric ceramic to generate displacement and push the sample loading stage by the connecting base. The invention coordinating with high resolution TEM realizes the observation of the microstructure in atomic and even sub angstrom scales, and at the same time it ensures the controllable deformation of nanomaterials, further realizes the integrative research on the material microstructure-mechanical properties and reveals the deformation mechanism of the materials.
机译:基于压电陶瓷驱动的TEM双倾斜原位机械式样品支架属于材料微观结构-机械性能原位表征领域,它由样品支架轴体和压电陶瓷驱动系统两部分组成。样品架轴主体包括倾斜台,样品架,线性步进电机,驱动杆,驱动连杆。压电陶瓷驱动系统包括压电陶瓷加载台,压电陶瓷,连接基座和实现拉伸或压缩功能的样品加载台。样品在X和Y轴方向上的双轴倾斜是通过线性步进电机驱动的驱动杆的往复运动实现的。样品的拉伸或压缩是通过在压电陶瓷上施加电压以产生位移并通过连接基座推动样品加载台来实现的。本发明与高分辨率TEM配合,实现了对原子级甚至亚埃级微观结构的观察,同时保证了纳米材料可控的形变,进一步实现了材料微观结构力学性能的综合研究,揭示了形变。材料的机理。

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