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Method for preparing structured graphene on SiC substrate based on Cl2 reaction

机译:基于Cl 2 反应在SiC衬底上制备结构化石墨烯的方法

摘要

Disclosed is a method for preparing structured graphene on a SiC substrate on the basis of Cl2 reaction, the procedures are as follows: firstly, performing standard cleaning to a SiC sample chip; depositing a layer of SiO2 on the surface of the SiC sample chip and engraving a figure window on the SiO2 layer; then arranging the windowed sample chip in a quartz tube, introducing a mixed gas of Ar and Cl2 into the quartz tube, reacting the bare SiC with Cl2 for 3-8 min at 700-1100° C. to generate a carbon film; arranging the generated carbon film in Ar gas, annealing for 10-30 min at 1000-1200° C. to generate the structured graphene on the window on the carbon film. The method is simple and safe; the generated structured graphene has a smooth surface and low porosity and can be used for making microelectronic devices.
机译:本发明公开了一种基于Cl 2 反应在SiC衬底上制备结构化石墨烯的方法,其步骤如下:首先,对SiC样品芯片进行标准清洗。在SiC样品芯片的表面上沉积SiO 2 层,并在SiO 2 层上刻出图形窗口。然后将开窗样品芯片放在石英管中,将Ar和Cl 2 的混合气体引入石英管,使裸露的SiC与Cl 2 反应3-8在700-1100℃下进行至少1分钟以产生碳膜;将生成的碳膜排列在氩气中,在1000-1200℃下退火10-30分钟,以在碳膜的窗口上生成结构化的石墨烯。该方法简单安全。生成的结构化石墨烯表面光滑,孔隙率低,可用于制造微电子器件。

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