The invention concerns a method for treating a hydrocarbon feed gas stream containing at least CO2 and H2S to recover a high quality purified CO2 gas stream, comprising the following steps: a. separating said hydrocarbon feed gas stream into (i) a sweetened hydrocarbon gas stream, and (ii) an acid gas stream comprising at least CO2 and H2S; b. introducing said gas stream (ii) into a Claus unit, thereby recovering (iii) a liquid stream of elemental sulfur and (iv) a tail gas mainly comprising N2, CO2, SO2 and H2S; c. introducing the tail gas (iv) into a hydrogenation reactor and then into a quench contactor of the Tail Gas Treatment Unit (TGTU) thereby recovering (v) a hydrogenated tail gas stream mainly comprising N2, H2, CO, CO2 and H2S; d. contacting said tail gas stream (v) with a non-selective amine-based solvent into a non-selective acid gas absorption unit of the TGTU thereby recovering (vi) an off gas mainly comprising N2, H2 and CO and (vii) a gas stream enriched in CO2 and H2S; e. sending the off gas (vi) to an incinerator; f. contacting said enriched gas stream (vii) with a selective H2S-absorption solvent into a selective H2S-absorption unit thereby recovering (viii) a highly purified CO2 gas stream and (ix) a H2S-enriched gas stream, as well as the device for carrying said method.
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