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Proton ionic liquid of tebuconazole and method for producing them

机译:戊唑醇的质子离子液体及其生产方法

摘要

the subject invention are proton ion liquids of general formula 1, in which kationem is tebuconazole, and organic anion from fenoksykwasu00f3w and their manufacture. liquids are applicable as fungicidal compounds and herbicides.process for the production of ionic liquids is that tebuconazole of the general formula (2), shall be subjected to the reaction with the organic acid with the mole ratio of tebuconazole to organic acid equal to 1: 0.8 - 1.5 in an alcohol or aromatic hydrocarbons, or chlorowcopochodnych, or es tru00f3w ketones or aldehydes, or, advantageously, alcohol, at a temperature from 273 to 363 k, during 1 - 48 hafter which the vaporized solvent, and the residue is washed with hexane to remove excess unreacted acid. then the residue dried under reduced pressure at 303 to 343 k, during the 4 - 12 hours.
机译:本发明是通式1的质子离子液体,其中kationem是戊唑醇,以及来自fenoksykwas的有机阴离子及其制造。液体可用作杀真菌化合物和除草剂。生产离子液体的方法是,将通式(2)的戊唑醇与有机酸进行反应,其中戊唑醇与有机酸的摩尔比等于1:在1-48小时内,在温度为273至363 k的醇或芳族烃,或chlorowcopochodnych或es tr u00f3w酮或醛,或优选为醇的溶液中为0.8- 1.5,此后蒸发溶剂和残留物用己烷洗涤以除去过量的未反应的酸。然后将残余物在303至343 k减压下干燥4至12小时。

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