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- PREPARATION METHOD OF POLYLACTIC ACID BY ONE-POT DIRECT POLYCONDENSATION

机译:-一锅法直接缩聚制备聚乳酸的方法

摘要

The present invention relates to a method for producing polylactic acid, which comprises one-port direct polymerization comprising lactic acid selected from L-lactic acid, D-lactic acid or a mixture thereof in a screw polymerization reactor, and specifically, to a method for producing polylactic acid, in which the one-port direct polymerization comprises a melt polymerization step, a half crystallization step and a solid phase polymerization step, and the polylactic acid is dehydrated by high-temperature decompression with a vacuum pump during the one-port direct polymerization. It is an object of the present invention to provide the polylactic acid having a high molecular weight by performing polymerization with a single polymerization reactor without intermediate purification, recovery and grinding steps of lactic acid by the one-port direct polymerization.
机译:聚乳酸的制造方法技术领域本发明涉及一种在螺杆式聚合反应器中进行包含选自L-乳酸,D-乳酸或其混合物的乳酸的单端口直接聚合的聚乳酸的制造方法,特别涉及制备聚乳酸,其中单端口直接聚合包括熔融聚合步骤,半结晶步骤和固相聚合步骤,并且在单端口直接过程中通过真空泵的高温减压使聚乳酸脱水聚合。本发明的目的是提供一种高分子量的聚乳酸,其通过在一个聚合反应器中进行聚合而无需通过单端口直接聚合进行乳酸的中间纯化,回收和研磨步骤。

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