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method for manufacturing amorphous nano-sized ceramic powder

机译:非晶态纳米陶瓷粉的制备方法

摘要

The present invention relates to a method of preparing an amorphous nano-sized ceramic powder, and more specifically, to a method of preparing an amorphous nano-sized ceramic powder, the method which is capable of increasing reaction speed of a mixed aqueous solution as well as solubility of a prepared noncrystalline. The method of the present invention comprises: a first step of moving a calcium hydroxide (Ca(OH)_2) powder to a three-neck flask of an atmosphere that does not contain carbon dioxide and adding distilled water to the calcium hydroxide (Ca(OH)_2) powder twice or more to prepare an aqueous calcium hydroxide (Ca(OH)_2) solution, and injecting a phosphoric acid (H_3PO_4) solution into another three-neck flask of an atmosphere that does not contain carbon dioxide and adding distilled water to the phosphoric acid (H_3PO_4) solution twice or more to prepare an aqueous phosphoric acid (H_3PO_4) solution; a second step of moving the aqueous calcium hydroxide (Ca(OH)_2) solution and the aqueous phosphoric acid (H_3PO_4) solution to a main reactor in the same rate and volume to react a mixture of the aqueous calcium hydroxide (Ca(OH)_2) solution and the aqueous phosphoric acid (H_3PO_4) solution in the main reactor of an atmosphere that does not contain carbon dioxide; and a third step of drying the main reactor of an atmosphere that does not contain carbon dioxide to prepare a nano-sized ceramic powder.
机译:本发明涉及一种非晶态纳米尺寸陶瓷粉末的制备方法,更具体地,涉及一种非晶态纳米尺寸陶瓷粉末的制备方法,该方法还能够提高混合水溶液的反应速度。制备的非晶态的溶解度。本发明的方法包括:第一步,将氢氧化钙(Ca(OH)_2)粉末移至不包含二氧化碳的气氛的三颈烧瓶中,并向氢氧化钙(Ca( OH)_2)粉末两次或更多次,以制备氢氧化钙(Ca(OH)_2)水溶液,然后将磷酸(H_3PO_4)溶液注入另一个不含二氧化碳的气氛的三颈烧瓶中,并加入蒸馏水向磷酸(H_3PO_4)溶液中加水两次或更多次以制备磷酸(H_3PO_4)水溶液。第二步是将氢氧化钙(Ca(OH)_2)水溶液和磷酸(H_3PO_4)水溶液以相同的速率和体积移至主反应器,以使氢氧化钙(Ca(OH))的混合物反应_2)溶液和主反应器中的磷酸水溶液(H_3PO_4)不含二氧化碳。第三步是在不包含二氧化碳的气氛中干燥主反应器以制备纳米尺寸的陶瓷粉末。

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