首页> 外国专利> METHOD FOR OBTAINING ALCOXY-HYDROXYBENZALDEHYDE, THAT IS SUBSTANTIALLY FREE OF ALKYL-ALCOXY-HYDROXYBENZALDEHYDE

METHOD FOR OBTAINING ALCOXY-HYDROXYBENZALDEHYDE, THAT IS SUBSTANTIALLY FREE OF ALKYL-ALCOXY-HYDROXYBENZALDEHYDE

机译:获得基本上不含烷基-羟基-羟基苯甲醛的羟基-羟基苯甲醛的方法

摘要

FIELD: technological processes.;SUBSTANCE: present invention relates to a process of the production of at least one alkoxyhydroxybenzaldehyde ("AHBA") which can be used as a flavor or perfume, and also as an intermediate from at least one hydroxyphenol ("HP"). Method includes the step of forming at least one alkoxyphenol ("AP") and alkyl alkoxyphenol ("AAP") and the step of separating (S) AP from AAP, the separation step (S) being carried out before obtaining AHBA, the AHBA compound is prepared by attaching an aldehyde group to the AP compound by condensation with glyoxylic acid, followed by oxidation of the resulting compound, and the separation step (S) is carried out before oxidation to form an AHBA compound. Invention also relates to a method for separating guaiacol (GA) and/or gvetol (GE) from a mixture containing GA and/or GE and a process for synthesizing at least one AP in the vapor phase.;EFFECT: proposed method makes it possible to obtain AHBA with high purity and good yield with high conversion of HP.;17 cl, 4 dwg, 3 ex
机译:制备至少一种烷氧基羟基苯甲醛(“ AHBA”)的方法,所述烷氧基羟基苯甲醛可以用作调味剂或香料,还可以由至少一种羟基酚(“ HP ”)。该方法包括形成至少一种烷氧基苯酚(“ AP”)和烷基烷氧基苯酚(“ AAP”)的步骤以及从AAP分离(S)AP的步骤,分离步骤(S)在获得AHBA之前进行,所述AHBA通过与乙醛酸缩合使醛基与AP化合物连接,然后氧化所得化合物,制备化合物,然后在氧化之前进行分离步骤(S)以形成AHBA化合物。本发明还涉及一种从含有GA和/或GE的混合物中分离愈创木酚(GA)和/或甲萘酚(GE)的方法,以及一种在气相中合成至少一种AP的方法。效果:所提出的方法使得它成为可能。以获得高纯度,高收率和高HP转化率的AHBA。; 17 cl,4 dwg,3 ex

著录项

  • 公开/公告号RU2648044C2

    专利类型

  • 公开/公告日2018-03-22

    原文格式PDF

  • 申请/专利权人 RODIA OPERASON;

    申请/专利号RU20150106362

  • 发明设计人 GAREL LORAN;GAJE YUBER;

    申请日2013-07-12

  • 分类号C07C45/54;C07C47/575;C07C47/58;C07C51/367;C07C65/21;C07C41/01;C07C41/42;C07C43/23;

  • 国家 RU

  • 入库时间 2022-08-21 12:35:42

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