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METHOD FOR WATER-SOLUBLE FRACTIONATION OF HUMUS, PARTICULARLY FRACTIONATION OF BROWN HUMIC ACIDS, FROM A SOIL SAMPLE

机译:土壤样品中腐殖质的水分离法,特别是棕腐殖酸的水分离法

摘要

FIELD: chemistry.;SUBSTANCE: invention relates to soil sciences, agricultural chemistry and pharmaceutical industry, namely to a method for fractionation of brown humic acids. Method for fractionation of brown humic acids from a soil sample, comprising drying, grinding, removing organic residues and screening a soil sample, alkaline extraction of a soil lot with a solution of 0.1 N NaOH, the resultant alkaline extract is further mixed five times every 2 minutes at a speed of w=60 rpm, followed by shaking it for 10 minutes every time with a shaking frequency of f=60 cycles/min, and the separation of the alkaline extract from the soil particles is carried out by settling it for 120 minutes, wherein sampling from the alkaline extract is carried out directly from the process vessel, in which the entire process of fractionation of brown humic acids from a soil sample is carried out.;EFFECT: above described method provides shorter time of fractionation of brown humic acids and higher accuracy of determination.;1 cl, 1 dwg, 1 tbl, 2 ex
机译:棕色腐殖酸的分馏方法技术领域本发明涉及土壤科学,农业化学和制药工业,即一种棕色腐殖酸的分馏方法。从土壤样品中分离棕色腐殖酸的方法,包括干燥,研磨,去除有机残留物和筛分土壤样品,用0.1N NaOH溶液碱提取土壤块,然后将所得碱提取物进一步混合5次以w = 60 rpm的速度离心2分钟,然后每次以f = 60转/分钟的振摇频率振摇10分钟,然后通过将其沉淀下来,从土壤颗粒中分离出碱性提取物120分钟,其中从碱提取液中直接从处理容器中取样,在该处理容器中,从土壤样品中分离棕色腐殖酸的整个过程都进行了;效果:上述方法提供了更短的棕色分离时间腐殖酸和更高的测定精度。; 1 cl,1 dwg,1 tbl,2 ex

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