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IMPROVED COUPLING METHOD FOR PEPTIDE SYNTHESIS AT ELEVATED TEMPERATURES
IMPROVED COUPLING METHOD FOR PEPTIDE SYNTHESIS AT ELEVATED TEMPERATURES
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机译:高温下多肽合成的改进偶联方法
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摘要
An improved method for coupling carboxylic acids and amines is disclosed that includes the steps of combining a hyper-acid sensitive linker connecting an amine and a resin, a carboxylic acid, a carbodiimide, an activator additive, and a base, and carrying out the activation and coupling at a temperature greater than 30°C.
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