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METHOD FOR PREPARING OIL-SOLUBLE TUNGSTEN DISULFIDE NANOSHEET

机译:制备油溶性二硫化钨纳米片的方法

摘要

Provided is a method for preparing an oil-soluble tungsten disulfide nanosheet, comprising: by using tungsten hexachloride as a tungsten source, and thioacetamide and thiourea as active sulfur sources, conducting a constant-temperature reaction at 100-200°C for 60 minutes or more in the presence of a surface modifier, wherein the surface modifier is at least one of straight-chain or branched-chain fatty acid or fatty amine of which the number of carbon atoms is 6-40. By means of the method, no ion needing to be removed is introduced into a reaction system, and no toxic pollutant is discharged; the synthesis process temperature is low; the prepared oil-soluble tungsten disulfide nanosheet has uniform particle size, good oil dissolubility, and a wide application prospect in the fields of lubricating oil nano-additives, etc.
机译:本发明提供一种油溶性二硫化钨纳米片的制备方法,其包括:以六氯化钨为钨源,以硫代乙酰胺和硫脲为活性硫源,在100-200℃下进行60分钟恒温反应,或在表面改性剂的存在下,其中所述表面改性剂为碳原子数为6-40的直链或支链脂肪酸或脂肪胺中的至少一种。通过该方法,不需要去除的离子被引入到反应系统中,并且没有毒性污染物被排放。合成过程温度低;制备的油溶性二硫化钨纳米片粒径均匀,油溶性好,在润滑油纳米添加剂领域等具有广阔的应用前景。

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