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CORE-SHELL TYPE GOLD-RUTHENIUM OXIDE NANO-COMPOSITE MATERIAL AND PREPARATION METHOD THEREFOR

机译:核壳型氧化金-氧化钌纳米复合材料及其制备方法

摘要

A core-shell type gold-ruthenium oxide nano-composite material, comprising gold nanoparticles in a core and ruthenium oxide coated on the outside thereof, the molar ratio of the gold nanoparticles to the ruthenium oxide being 1:0.2-0.8. The preparation method for the core-shell type gold-ruthenium oxide nano-composite material comprises steps of: adjusting the pH of a gold-containing solution to 8-12, and adding an organic solution of ruthenium acetylacetonate and then uniformly mixing the same, the gold-containing solution comprising gold nanoparticles, a cationic surfactant, and water, the concentration of the cationic surfactant in the gold-containing solution being 0.05 × 10-3 to 1.5 × 10-3 mol/L; and carrying out a hydrothermal reaction in the mixed solution at 100-120°C to obtain a core-shell type gold-ruthenium oxide nano-composite material.
机译:核-壳型金-氧化钌纳米复合材料,包括核中的金纳米颗粒和涂覆在其外侧的氧化钌,金纳米颗粒与氧化钌的摩尔比为1:0.2-0.8。核-壳型金-钌氧化物纳米复合材料的制备方法包括以下步骤:将含金溶液的pH调节至8-12,加入乙酰丙酮钌钌的有机溶液,然后均匀混合。包含金纳米颗粒,阳离子表面活性剂和水的含金溶液,该含金溶液中阳离子表面活性剂的浓度为0.05×10 -3 至1.5×10 -3 mol / L;然后在混合溶液中于100-120℃进行水热反应,得到核-壳型金-氧化钌纳米复合材料。

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