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QUINONE ANALYSIS METHOD AND ONLINE SFE-SFC SYSTEM FOR IMPLEMENTING SAID METHOD

机译:实施方法的醌类分析方法和在线SFE-SFC系统

摘要

This quinone analysis method comprises: a sample sealing step for sealing a sample including quinones in an extraction container; an extraction step for, after the sample sealing step and as a series of extraction operations, carrying out "static extraction" in which a first mobile phase solvent for extracting components including quinones from the sample is supplied from a mobile phase supply unit to the extraction container and the extraction container is left still in a state of being filled with the first mobile phase solvent, and then carrying out "dynamic extraction" in which the first mobile phase solvent including components extracted from the sample is allowed to flow through the analysis column and at least the components including quinones from among the components included in the first mobile phase solvent are captured by the analysis column; and an analysis step for supplying, from the mobile phase supply unit, a second mobile phase solvent for eluting, from the analysis column, the components captured by the analysis column as a result of the series of extraction operations, causing the second mobile phase solvent to flow through the analysis column, separating and eluting the components captured by the analysis column, and detecting the same using a detector.
机译:该醌分析方法包括:样品密封步骤,用于将包含醌的样品密封在提取容器中;和萃取步骤,用于在样品密封步骤之后并且作为一系列萃取操作,执行“静态萃取”,其中将用于从样品中萃取包括醌的组分的第一流动相溶剂从流动相供应单元中提供给萃取容器和提取容器在填充有第一流动相溶剂的状态下保持静止,然后执行“动态提取”,使包括从样品中提取的成分的第一流动相溶剂流过分析柱第一流动相溶剂所含的成分中,至少包含醌的成分被分析柱捕获。分析步骤,用于从所述流动相供应单元中供应第二流动相溶剂,所述第二流动相溶剂用于从所述分析柱洗脱由于一系列提取操作而被所述分析柱捕获的组分,从而导致所述第二流动相溶剂流入分析柱,分离并洗脱分析柱捕获的组分,并使用检测器进行检测。

著录项

  • 公开/公告号WO2019163245A1

    专利类型

  • 公开/公告日2019-08-29

    原文格式PDF

  • 申请/专利权人 SHIMADZU CORPORATION;

    申请/专利号WO2018JP44126

  • 发明设计人 MATSUMOTO KEIKO;

    申请日2018-11-30

  • 分类号G01N30/02;B01D15/12;B01D15/16;B01D15/40;B01D15/42;B01J20/281;B01J20/287;G01N30/06;G01N30/26;G01N30/34;

  • 国家 WO

  • 入库时间 2022-08-21 11:53:28

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