首页> 外国专利> MAGNESIUM OXIDE WHISKER IN-SITU SYNTHESIS SPINEL-REINFORCED MAGNESIUM OXIDE-BASED CRUCIBLE AND PREPARATION METHOD THEREFOR

MAGNESIUM OXIDE WHISKER IN-SITU SYNTHESIS SPINEL-REINFORCED MAGNESIUM OXIDE-BASED CRUCIBLE AND PREPARATION METHOD THEREFOR

机译:氧化镁晶须原位合成尖晶石增强的氧化镁坩埚及其制备方法

摘要

A magnesium oxide whisker in-situ synthesis spinel-reinforced magnesium oxide-based crucible that may perform sintering at a low temperature and that has excellent chemical stability and thermal shock resistance, and a preparation method therefor, the preparation method comprising the following steps: (1) according to mass percentage, mixing 15%-25% of nano alumina sol and 0.8%-1.5% of a rheological agent, the rest being magnesium oxide ceramic powder containing a nano titanium dioxide sintering aid, adding anhydrous ethanol, mixing evenly by means of ball milling, and then preparing a ceramic slurry having a solid content of 65%-75%; (2) preparing a crucible biscuit; (3) preparing a crucible blank; (4) placing the magnesium oxide-based crucible blank in alumina sol for vacuum impregnation treatment, then performing surface finishing treatment, drying, then performing high-temperature secondary sintering at a temperature of 1350°C-1550°C, and cooling to room temperature in the furnace to obtain a magnesium oxide-based crucible.
机译:可以在低温下烧结并且具有优异的化学稳定性和耐热冲击性的氧化镁晶须原位合成尖晶石增强的氧化镁基坩埚及其制备方法,该制备方法包括以下步骤:( 1)按质量百分比,将15%-25%的纳米氧化铝溶胶和0.8%-1.5%的流变剂混合,其余为含有纳米二氧化钛烧结助剂的氧化镁陶瓷粉末,加入无水乙醇,通过球磨的方法,然后制备固体含量为65%-75%的陶瓷浆料; (2)准备坩埚饼干; (3)准备坩埚坯料; (4)将氧化镁类坩埚坯料放入氧化铝溶胶中进行真空浸渍处理,然后进行表面处理,干燥,然后在1350℃至1550℃的温度下进行高温二次烧结,并冷却至室温。在熔炉中加热温度,以获得基于氧化镁的坩埚。

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