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1166--25--16- Method of Preparing 1166-tetrachloro-25-dioxa-16-diphoshexane

机译:1166--25--16-制备方法1166-四氯-25-二氧杂-16-二磷己烷

摘要

A method for manufacturing 1,1,6,6-tetrachloro-2,5-dioxa-1,6-diphoshexane according to the present invention is the method for manufacturing 1,1,6,6-tetrachloro-2,5-dioxa-1,6-diphoshexane represented by chemical formula 2 by phosphorylation of an ethylene glycol compound represented by chemical formula 1 in the presence of an organic base. The method has effects of having an easy manufacturing process, being able to mass produce, obtaining 1,1,6,6-tetrachloro-2,5-dioxa-1,6-diphoshexane in a high yield, and manufacturing 1,1,6,6-tetrachloro-2,5-dioxa-1,6-diphoshexane with the high yield and a high purity.
机译:根据本发明的制造1,1,6,6-四氯-2,5-二氧杂-1,6-二磷己烷的方法是制造1,1,6,6-四氯-2,5-二氧杂的方法。在有机碱的存在下,通过化学式1表示的乙二醇化合物的磷酸化,化学式2表示的-1,6-二磷己烷。该方法具有易于制造的过程,能够大量生产,以高收率获得1,1,6,6-四氯-2,5-二氧杂-1,6-二磷己烷并制造1,1,1,3,3,4,5,5,5,5,4,5,4,5,7,8,8,10,12,13-具有高收率和高纯度的6,6-四氯-2,5-二氧杂-1,6-二磷己烷。

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